4-chloro-α-[4-(4,5-dihydro-4,4-dimethyl-2-oxazolyl)phenyl]-benzenemethanol

Base Information

Chemical Name:4-chloro-α-[4-(4,5-dihydro-4,4-dimethyl-2-oxazolyl)phenyl]-benzenemethanol
CAS No.:211388-40-8
Molecular Formula:C₁₈H₁₈ClNO₂
Molecular Weight:315.799
Hs Code.:

Synonyms:4-chloro-α-[4-(4,5-dihydro-4,4-dimethyl-2-oxazolyl)phenyl]-benzenemethanol

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Chemical Property of 4-chloro-α-[4-(4,5-dihydro-4,4-dimethyl-2-oxazolyl)phenyl]-benzenemethanol

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Technology Process of 4-chloro-α-[4-(4,5-dihydro-4,4-dimethyl-2-oxazolyl)phenyl]-benzenemethanol

There total 3 articles about 4-chloro-α-[4-(4,5-dihydro-4,4-dimethyl-2-oxazolyl)phenyl]-benzenemethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 32664-14-5
2-(4-bromophenyl)-4,4-dimethyl-2-oxazoline

: 104-88-1
4-chlorobenzaldehyde

: 211388-40-8
4-chloro-α-[4-(4,5-dihydro-4,4-dimethyl-2-oxazolyl)phenyl]-benzenemethanol

Guidance literature:: 2-(4-bromophenyl)-4,4-dimethyl-2-oxazoline; With magnesium; In tetrahydrofuran; for 1.5h; Heating;

4-chlorobenzaldehyde; In tetrahydrofuran; for 2.5h; Heating;

Reference yield:

: 33708-69-9
4-bromo-N-[2-(2-methyl-2-propan-1-ol)]benzamide

: 211388-40-8
4-chloro-α-[4-(4,5-dihydro-4,4-dimethyl-2-oxazolyl)phenyl]-benzenemethanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: 60 percent / thionyl chloride / toluene; CH₂Cl₂ / 72 h / 20 °C

2.1: Mg / tetrahydrofuran / 1.5 h / Heating

2.2: 53 percent / tetrahydrofuran / 2.5 h / Heating

With thionyl chloride; magnesium; In tetrahydrofuran; dichloromethane; toluene;

Reference yield:

: 586-75-4
4-chlorobenzoyl chloride

: 211388-40-8
4-chloro-α-[4-(4,5-dihydro-4,4-dimethyl-2-oxazolyl)phenyl]-benzenemethanol

Guidance literature:: Multi-step reaction with 3 steps

1.1: 82 percent / CH₂Cl₂ / 24 h / 20 °C

2.1: 60 percent / thionyl chloride / toluene; CH₂Cl₂ / 72 h / 20 °C

3.1: Mg / tetrahydrofuran / 1.5 h / Heating

3.2: 53 percent / tetrahydrofuran / 2.5 h / Heating

With thionyl chloride; magnesium; In tetrahydrofuran; dichloromethane; toluene;