3-benzylpenta-3,4-dienyl sulfamate

Base Information

Chemical Name:3-benzylpenta-3,4-dienyl sulfamate
CAS No.:1202756-85-1
Molecular Formula:C₁₂H₁₅NO₃S
Molecular Weight:253.322
Hs Code.:

Synonyms:3-benzylpenta-3,4-dienyl sulfamate

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Chemical Property of 3-benzylpenta-3,4-dienyl sulfamate

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Technology Process of 3-benzylpenta-3,4-dienyl sulfamate

There total 1 articles about 3-benzylpenta-3,4-dienyl sulfamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 7778-42-9
sulphamoyl chloride

: 821783-05-5
3-benzylpenta-3,4-dien-1-ol

: 1202756-85-1
3-benzylpenta-3,4-dienyl sulfamate

Guidance literature:: sulphamoyl chloride; With formic acid; In acetonitrile; at 0 - 21 ℃; Inert atmosphere;

3-benzylpenta-3,4-dien-1-ol; With 2,6-dimethylpyridine; In N,N-dimethyl acetamide; acetonitrile; at -5 - 0 ℃; for 2h; Inert atmosphere;

Reference yield: 67.0%

: para-methoxyphenylmagnesium bromide lithium chloride

: 1202756-85-1
3-benzylpenta-3,4-dienyl sulfamate

: 7-benzyl-1-(4-methoxyphenyl)-4-oxa-3-thia-2-azabicyclo[5.1.0]octane 3,3-dioxide

Guidance literature:: 3-benzylpenta-3,4-dienyl sulfamate; With bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]}; bis(tertbutylcarbonyloxy)iodobenzene; In α,α,α-trifluorotoluene; at 45 ℃; for 3h; Inert atmosphere;

para-methoxyphenylmagnesium bromide lithium chloride; In tetrahydrofuran; α,α,α-trifluorotoluene; at -30 - 0 ℃; for 19h; Inert atmosphere;

Reference yield: 52.0%

: 1202756-85-1
3-benzylpenta-3,4-dienyl sulfamate

: 1826-67-1
vinyl magnesium bromide

: 7-benzyl-1-vinyl-4-oxa-3-thia-2-azabicyclo[5.1.0]octane 3,3-dioxide

Guidance literature:: 3-benzylpenta-3,4-dienyl sulfamate; With bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]}; bis(tertbutylcarbonyloxy)iodobenzene; In α,α,α-trifluorotoluene; at 45 ℃; for 3h; Inert atmosphere;

vinyl magnesium bromide; In tetrahydrofuran; α,α,α-trifluorotoluene; at -30 - 0 ℃; for 19h; Inert atmosphere;