1-(4-methoxy-phenyl)-2-(4,4,6-trimethyl-5,6-dihydro-4H-[1,3]oxazin-2-yl)-ethanol

Base Information

Chemical Name:1-(4-methoxy-phenyl)-2-(4,4,6-trimethyl-5,6-dihydro-4H-[1,3]oxazin-2-yl)-ethanol
CAS No.:86657-69-4
Molecular Formula:C₁₆H₂₃NO₃
Molecular Weight:277.364
Hs Code.:

1-(4-methoxy-phenyl)-2-(4,4,6-trimethyl-5,6-dihydro-4<i>H</i>-[1,3]oxazin-2-yl)-ethanol

Synonyms:1-(4-methoxy-phenyl)-2-(4,4,6-trimethyl-5,6-dihydro-4H-[1,3]oxazin-2-yl)-ethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4-methoxy-phenyl)-2-(4,4,6-trimethyl-5,6-dihydro-4H-[1,3]oxazin-2-yl)-ethanol

Chemical Property:

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Technology Process of 1-(4-methoxy-phenyl)-2-(4,4,6-trimethyl-5,6-dihydro-4H-[1,3]oxazin-2-yl)-ethanol

There total 1 articles about 1-(4-methoxy-phenyl)-2-(4,4,6-trimethyl-5,6-dihydro-4H-[1,3]oxazin-2-yl)-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 26939-18-4
2,4,4,6-tetramethyl-5,6-dihydro-4H-1,3-oxazine

: 123-11-5
4-methoxy-benzaldehyde

: 86657-69-4
1-(4-methoxy-phenyl)-2-(4,4,6-trimethyl-5,6-dihydro-4H-[1,3]oxazin-2-yl)-ethanol

Guidance literature:: Multistep reaction; (i) nBuLi, THF, (ii) /BRN= 471382/;
DOI:10.1021/ja01031a054

Reference yield:

: 86657-69-4
1-(4-methoxy-phenyl)-2-(4,4,6-trimethyl-5,6-dihydro-4H-[1,3]oxazin-2-yl)-ethanol

: 1963-36-6
4-methoxycinnamaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄, HCl, NaOH / tetrahydrofuran; aq. ethanol / 1 h / -40 - -35 °C / pH=7

2: oxalic acid dihydrate / H₂O / 2 h / Heating

With hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; oxalic acid; In tetrahydrofuran; ethanol; water;
DOI:10.1002/ardp.19833160619

Reference yield:

: 86657-69-4
1-(4-methoxy-phenyl)-2-(4,4,6-trimethyl-5,6-dihydro-4H-[1,3]oxazin-2-yl)-ethanol

: 1-(4-methoxy-phenyl)-2-(4,4,6-trimethyl-[1,3]oxazinan-2-yl)-ethanol

Guidance literature:: With hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; In tetrahydrofuran; ethanol; at -40 - -35 ℃; for 1h; pH=7;
DOI:10.1002/ardp.19833160619