dimethyl [5-(benzyloxy)-1-(biphenyl-3-yl)-4-oxo-1,4-dihydropyridin-3-yl]boronate

Base Information

Chemical Name:dimethyl [5-(benzyloxy)-1-(biphenyl-3-yl)-4-oxo-1,4-dihydropyridin-3-yl]boronate
CAS No.:1333331-83-1
Molecular Formula:C₂₆H₂₄BNO₄
Molecular Weight:425.292
Hs Code.:

Synonyms:dimethyl [5-(benzyloxy)-1-(biphenyl-3-yl)-4-oxo-1,4-dihydropyridin-3-yl]boronate

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Chemical Property of dimethyl [5-(benzyloxy)-1-(biphenyl-3-yl)-4-oxo-1,4-dihydropyridin-3-yl]boronate

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Technology Process of dimethyl [5-(benzyloxy)-1-(biphenyl-3-yl)-4-oxo-1,4-dihydropyridin-3-yl]boronate

There total 7 articles about dimethyl [5-(benzyloxy)-1-(biphenyl-3-yl)-4-oxo-1,4-dihydropyridin-3-yl]boronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121-43-7,63156-11-6
Trimethyl borate

: 1333331-82-0
3-(benzyloxy)-1-(biphenyl-3-yl)-5-bromopyridin-4(1H)-one

: 1333331-83-1
dimethyl [5-(benzyloxy)-1-(biphenyl-3-yl)-4-oxo-1,4-dihydropyridin-3-yl]boronate

Guidance literature:: 3-(benzyloxy)-1-(biphenyl-3-yl)-5-bromopyridin-4(1H)-one; With isopropylmagnesium chloride; lithium chloride; In tetrahydrofuran; at -10 - 25 ℃;

Trimethyl borate; In tetrahydrofuran; for 3.5h;

Reference yield:

: 1219-33-6
5-(benzyloxy)-4-oxo-4H-pyran-2-carboxylic acid

: 1333331-83-1
dimethyl [5-(benzyloxy)-1-(biphenyl-3-yl)-4-oxo-1,4-dihydropyridin-3-yl]boronate

Guidance literature:: Multi-step reaction with 3 steps

1.1: diphenylether / 0.17 h / 250 °C

2.1: N-Bromosuccinimide / acetic acid / 1 h / 18 - 25 °C

3.1: isopropylmagnesium chloride; lithium chloride / tetrahydrofuran / -10 - 25 °C

3.2: 3.5 h

With N-Bromosuccinimide; isopropylmagnesium chloride; lithium chloride; In tetrahydrofuran; diphenylether; acetic acid;

Reference yield:

: 100-44-7
benzyl chloride

: 1333331-83-1
dimethyl [5-(benzyloxy)-1-(biphenyl-3-yl)-4-oxo-1,4-dihydropyridin-3-yl]boronate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydroxide / water; methanol / 4.5 h / Reflux

2.1: Jones reagent / acetone / 0 - 25 °C

3.1: diphenylether / 0.17 h / 250 °C

4.1: N-Bromosuccinimide / acetic acid / 1 h / 18 - 25 °C

5.1: isopropylmagnesium chloride; lithium chloride / tetrahydrofuran / -10 - 25 °C

5.2: 3.5 h

With N-Bromosuccinimide; Jones reagent; isopropylmagnesium chloride; lithium chloride; sodium hydroxide; In tetrahydrofuran; methanol; diphenylether; water; acetic acid; acetone;