C₄₅H₅₃N₅O₆

Base Information

Chemical Name:C₄₅H₅₃N₅O₆
CAS No.:1581709-49-0
Molecular Formula:C₄₅H₅₃N₅O₆
Molecular Weight:759.946
Hs Code.:

C<sub>45</sub>H<sub>53</sub>N<sub>5</sub>O<sub>6</sub>

Synonyms:C₄₅H₅₃N₅O₆

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Chemical Property of C₄₅H₅₃N₅O₆

Chemical Property:

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Technology Process of C₄₅H₅₃N₅O₆

There total 16 articles about C₄₅H₅₃N₅O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 39979-08-3
methyl 7-aminoheptanoate

: 1581709-53-6
C₃₇H₃₈N₄O₅

: 1581709-49-0
C₄₅H₅₃N₅O₆

Guidance literature:: With hydrogenchloride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 6h;
DOI:10.1021/jm401536b

Reference yield:

: 100-39-0
benzyl bromide

: 1581709-49-0
C₄₅H₅₃N₅O₆

Guidance literature:: Multi-step reaction with 12 steps

1.1: potassium carbonate / acetonitrile

2.1: n-butyllithium / tetrahydrofuran

3.1: palladium on activated charcoal; hydrogen / ethanol / 20 °C / 760.05 Torr

3.2: 0.25 h / 20 °C

3.3: 3 h / Reflux

4.1: nitric acid; acetic acid / 0.5 h / 70 °C

5.1: tin(II) chloride dihdyrate; hydrogenchloride / ethanol / 3 h / 80 °C

6.1: tert.-butylnitrite; trimethylsilylazide / acetonitrile / 13 h / 0 - 20 °C

7.1: chloro(pentamethylcyclopentadienyl)ruthenium(II) tetramer / N,N-dimethyl-formamide / 12 h / 20 °C

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

9.1: triethylamine / dichloromethane / 12.5 h / 0 - 20 °C

10.1: triethylamine / N,N-dimethyl-formamide / 12 h / 20 °C

11.1: lithium hydroxide; water / tetrahydrofuran / 12 h / 20 °C

12.1: hydrogenchloride; N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / dichloromethane / 6 h / 20 °C

With hydrogenchloride; n-butyllithium; tert.-butylnitrite; tin(II) chloride dihdyrate; chloro(pentamethylcyclopentadienyl)ruthenium(II) tetramer; trimethylsilylazide; palladium on activated charcoal; tetrabutyl ammonium fluoride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; hydrogen; nitric acid; potassium carbonate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 7.1: |Huisgen Cycloaddition;
DOI:10.1021/jm401536b

Reference yield:

: 1383717-80-3
2,4-bis-(benzyloxy)-5-isopropylaniline

: 1581709-49-0
C₄₅H₅₃N₅O₆

Guidance literature:: Multi-step reaction with 7 steps

1: tert.-butylnitrite; trimethylsilylazide / acetonitrile / 13 h / 0 - 20 °C

2: chloro(pentamethylcyclopentadienyl)ruthenium(II) tetramer / N,N-dimethyl-formamide / 12 h / 20 °C

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

4: triethylamine / dichloromethane / 12.5 h / 0 - 20 °C

5: triethylamine / N,N-dimethyl-formamide / 12 h / 20 °C

6: lithium hydroxide; water / tetrahydrofuran / 12 h / 20 °C

7: hydrogenchloride; N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / dichloromethane / 6 h / 20 °C

With hydrogenchloride; tert.-butylnitrite; chloro(pentamethylcyclopentadienyl)ruthenium(II) tetramer; trimethylsilylazide; tetrabutyl ammonium fluoride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 2: |Huisgen Cycloaddition;
DOI:10.1021/jm401536b