(E)-N'-(1-(3-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide-d3

Base Information

• Chemical Name: (E)-N'-(1-(3-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide-d3
• CAS No.: 1220985-72-7
• Molecular Formula: C₁₅H₁₆N₂O₂S
• Molecular Weight: 291.346
• Mol file: 1220985-72-7.mol

Synonyms:(E)-N'-(1-(3-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide-d3

Chemical Property of (E)-N'-(1-(3-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide-d3

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (E)-N'-(1-(3-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide-d3

There total 1 articles about (E)-N'-(1-(3-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide-d3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

Acetophenone-methyl-d3 (17537-31-4) + toluene-4-sulfonic acid hydrazide (1576-35-8) → (E)-N'-(1-(3-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide-d3 (1220985-72-7)

Guidance literature:

In methanol; for 0.5h; Reflux;

DOI:10.1039/b925590g

Reference yield:

(E)-N'-(1-(3-methoxyphenyl)ethylidene)-4-methylbenzenesulfonohydrazide-d3 (1220985-72-7) + (E)-4-methyl-N′-(1-phenylethylidene)benzenesulfonohydrazide (62460-99-5) + 4-methoxyphenylboronic acid (5720-07-0) → 1-(4-methoxyphenyl)-1-phenylethene (4333-75-9) + C15H12(2)H2O (1220985-74-9)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; oxygen; copper(l) chloride; lithium tert-butoxide; In 1,4-dioxane; at 70 ℃; for 3h;

DOI:10.1039/b925590g

upstream raw materials:

Acetophenone-methyl-d3

toluene-4-sulfonic acid hydrazide

Downstream raw materials:

1-(4-methoxyphenyl)-1-phenylethene

C₁₅H₁₂⁽²⁾H₂O