Technology Process of (Z)-3-iodo-N,N-diisopropyl-2,3-diphenylacrylamide
There total 3 articles about (Z)-3-iodo-N,N-diisopropyl-2,3-diphenylacrylamide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-iodo-succinimide; silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; trimethylpyruvic acid;
In
1,2-dichloro-ethane;
for 16h;
stereoselective reaction;
Inert atmosphere;
Heating;
Sealed tube;
DOI:10.1021/ol4015915
- Guidance literature:
-
Multi-step reaction with 3 steps
1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 20 °C / Inert atmosphere; Cooling
2: dichloromethane / 20 °C / Inert atmosphere
3: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; silver hexafluoroantimonate; trimethylpyruvic acid; N-iodo-succinimide / 1,2-dichloro-ethane / 16 h / Inert atmosphere; Heating; Sealed tube
With
N-iodo-succinimide; silver hexafluoroantimonate; oxalyl dichloride; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; N,N-dimethyl-formamide; trimethylpyruvic acid;
In
dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/ol4015915
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dichloromethane / 20 °C / Inert atmosphere
2: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; silver hexafluoroantimonate; trimethylpyruvic acid; N-iodo-succinimide / 1,2-dichloro-ethane / 16 h / Inert atmosphere; Heating; Sealed tube
With
N-iodo-succinimide; silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; trimethylpyruvic acid;
In
dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/ol4015915
