C₂₅H₂₆N₂O₅S

Base Information

Chemical Name:C₂₅H₂₆N₂O₅S
CAS No.:798564-43-9
Molecular Formula:C₂₅H₂₆N₂O₅S
Molecular Weight:466.558
Hs Code.:

C<sub>25</sub>H<sub>26</sub>N<sub>2</sub>O<sub>5</sub>S

Synonyms:C₂₅H₂₆N₂O₅S

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Chemical Property of C₂₅H₂₆N₂O₅S

Chemical Property:

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Technology Process of C₂₅H₂₆N₂O₅S

There total 9 articles about C₂₅H₂₆N₂O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2295-31-0
thiazoline-2,4-dione

: 798563-45-8
1-(3-isopropoxybenzyl)-4-chloromethyl-6,7-dimethoxyisoquinoline

: 798564-43-9
C₂₅H₂₆N₂O₅S

Guidance literature:: 1-(3-isopropoxybenzyl)-4-chloromethyl-6,7-dimethoxyisoquinoline; With sodium hydride; In tetrahydrofuran; DMF (N,N-dimethyl-formamide); at 20 - 50 ℃; for 2.08333h;

thiazoline-2,4-dione; In tetrahydrofuran; DMF (N,N-dimethyl-formamide); at 20 ℃; for 66h;

Reference yield:

: 93-17-4
3,4-dimethoxyphenylacetonitrile

: 798564-43-9
C₂₅H₂₆N₂O₅S

Guidance literature:: Multi-step reaction with 8 steps

1.1: ethanol; sodium / toluene / 2 h / 80 - 85 °C

1.2: 2 h / 80 °C

2.1: hydrogenchloride; hydrogen / palladium 10% on activated carbon / ethanol; water / 2844.39 Torr

3.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / dichloromethane / 20 °C

4.1: phosphorus pentachloride / dichloromethane / 0 - 20 °C

5.1: sulfur / 0.33 h / 165 °C

6.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Heating / reflux

7.1: methanesulfonyl chloride; triethylamine / dichloromethane / 0.33 h / 0 °C

7.2: 20 °C

8.1: sodium hydride / tetrahydrofuran; DMF (N,N-dimethyl-formamide) / 2.08 h / 20 - 50 °C

8.2: 66 h / 20 °C

With hydrogenchloride; lithium aluminium tetrahydride; ethanol; phosphorus pentachloride; hydrogen; sodium; sodium hydride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; sulfur; methanesulfonyl chloride; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; DMF (N,N-dimethyl-formamide); ethanol; dichloromethane; water; toluene;

Reference yield:

: 36848-69-8
ethyl 2-cyano-2-(3,4-dimethoxyphenyl)acetate

: 798564-43-9
C₂₅H₂₆N₂O₅S

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrogenchloride; hydrogen / palladium 10% on activated carbon / ethanol; water / 2844.39 Torr

2.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / dichloromethane / 20 °C

3.1: phosphorus pentachloride / dichloromethane / 0 - 20 °C

4.1: sulfur / 0.33 h / 165 °C

5.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Heating / reflux

6.1: methanesulfonyl chloride; triethylamine / dichloromethane / 0.33 h / 0 °C

6.2: 20 °C

7.1: sodium hydride / tetrahydrofuran; DMF (N,N-dimethyl-formamide) / 2.08 h / 20 - 50 °C

7.2: 66 h / 20 °C

With hydrogenchloride; lithium aluminium tetrahydride; phosphorus pentachloride; hydrogen; sodium hydride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; sulfur; methanesulfonyl chloride; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; DMF (N,N-dimethyl-formamide); ethanol; dichloromethane; water;