{(μ2-1,2-bis(dicyclohexylphosphino)ethane)(dimethylacetylenedicarboxylate)palladium(0)}

Base Information

Chemical Name:{(μ2-1,2-bis(dicyclohexylphosphino)ethane)(dimethylacetylenedicarboxylate)palladium(0)}
CAS No.:107730-84-7
Molecular Formula:C₃₂H₅₄O₄P₂Pd
Molecular Weight:671.146
Hs Code.:

Synonyms:{(μ2-1,2-bis(dicyclohexylphosphino)ethane)(dimethylacetylenedicarboxylate)palladium(0)}

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {(μ2-1,2-bis(dicyclohexylphosphino)ethane)(dimethylacetylenedicarboxylate)palladium(0)}

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Technology Process of {(μ2-1,2-bis(dicyclohexylphosphino)ethane)(dimethylacetylenedicarboxylate)palladium(0)}

There total 7 articles about {(μ2-1,2-bis(dicyclohexylphosphino)ethane)(dimethylacetylenedicarboxylate)palladium(0)} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 148572-28-5
{(μ2-1,2-bis(dicyclohexylphosphino)ethane)palladium(0)}2

: 762-42-5
dimethyl acetylenedicarboxylate

: 107730-84-7
{(μ2-1,2-bis(dicyclohexylphosphino)ethane)(dimethylacetylenedicarboxylate)palladium(0)}

: 148572-34-3
{(μ2-1,2-bis(dicyclohexylphosphino)ethane)(dimethylacetylenedicarboxylate)palladium(0)}2

Guidance literature:: In not given; at room temp. in toluene, THF or acetonitrile;;
DOI:10.1021/ja00062a087

Reference yield: 78.0%

: 107730-81-4,138663-39-5
[Pd((C₆H₁₁)2PCH₂CH₂P(C₆H₁₁)2)(C₄H₆)]

: 762-42-5
dimethyl acetylenedicarboxylate

: 107730-84-7
{(μ2-1,2-bis(dicyclohexylphosphino)ethane)(dimethylacetylenedicarboxylate)palladium(0)}

Guidance literature:: In diethyl ether; addn. of acetylene carboxylic acid to Pt complex in ether under Ar, room temp., 12h; filtration; evapn. to dryness; elem. anal.;