{(μ2-1,2-bis(dicyclohexylphosphino)ethane)(dimethylacetylenedicarboxylate)palladium(0)}2

Base Information

• Chemical Name: {(μ2-1,2-bis(dicyclohexylphosphino)ethane)(dimethylacetylenedicarboxylate)palladium(0)}2
• CAS No.: 148572-34-3
• Molecular Formula: C₆₄H₁₀₈O₈P₄Pd₂
• Molecular Weight: 1342.29

Synonyms:{(μ2-1,2-bis(dicyclohexylphosphino)ethane)(dimethylacetylenedicarboxylate)palladium(0)}2

Chemical Property of {(μ2-1,2-bis(dicyclohexylphosphino)ethane)(dimethylacetylenedicarboxylate)palladium(0)}2

Chemical Property:

Purity/Quality:

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Technology Process of {(μ2-1,2-bis(dicyclohexylphosphino)ethane)(dimethylacetylenedicarboxylate)palladium(0)}2

There total 3 articles about {(μ2-1,2-bis(dicyclohexylphosphino)ethane)(dimethylacetylenedicarboxylate)palladium(0)}2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

{(μ2-1,2-bis(dicyclohexylphosphino)ethane)palladium(0)}2 (148572-28-5) + dimethyl acetylenedicarboxylate (762-42-5) → {(μ2-1,2-bis(dicyclohexylphosphino)ethane)(dimethylacetylenedicarboxylate)palladium(0)} (107730-84-7) + {(μ2-1,2-bis(dicyclohexylphosphino)ethane)(dimethylacetylenedicarboxylate)palladium(0)}2 (148572-34-3)

Guidance literature:

In not given; at room temp. in toluene, THF or acetonitrile;;

DOI:10.1021/ja00062a087

Reference yield:

{H(μ2-1,2-bis(dicyclohexylphosphino)ethane)palladium(0)}2 → {(μ2-1,2-bis(dicyclohexylphosphino)ethane)(dimethylacetylenedicarboxylate)palladium(0)} (107730-84-7) + {(μ2-1,2-bis(dicyclohexylphosphino)ethane)(dimethylacetylenedicarboxylate)palladium(0)}2 (148572-34-3)

Guidance literature:

Multi-step reaction with 2 steps

1: not given

2: not given

In not given;

DOI:10.1021/ja00062a087

Reference yield:

Pd(C2O4)(1,2-bis(dicyclohexylphosphino)ethane) (141319-65-5) + dimethyl acetylenedicarboxylate (762-42-5) → {(μ2-1,2-bis(dicyclohexylphosphino)ethane)(dimethylacetylenedicarboxylate)palladium(0)} (107730-84-7) + {(μ2-1,2-bis(dicyclohexylphosphino)ethane)(dimethylacetylenedicarboxylate)palladium(0)}2 (148572-34-3)

Guidance literature:

In not given; Irradiation (UV/VIS); photolysis of the oxalate in the presence of excess DMAD;

DOI:10.1021/ja00062a087

upstream raw materials:

Pd(C₂O₄)(1,2-bis(dicyclohexylphosphino)ethane)

dimethyl acetylenedicarboxylate

{(μ2-1,2-bis(dicyclohexylphosphino)ethane)palladium(0)}2

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