8-Methoxy-11-oxo-5-(toluene-4-sulfonyl)-6,11-dihydro-5H-dibenzo[b,e]azepine-3-carbonyl chloride

Base Information

Chemical Name:8-Methoxy-11-oxo-5-(toluene-4-sulfonyl)-6,11-dihydro-5H-dibenzo[b,e]azepine-3-carbonyl chloride
CAS No.:78382-93-1
Molecular Formula:C₂₃H₁₈ClNO₅S
Molecular Weight:455.919
Hs Code.:

Synonyms:8-Methoxy-11-oxo-5-(toluene-4-sulfonyl)-6,11-dihydro-5H-dibenzo[b,e]azepine-3-carbonyl chloride

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Chemical Property of 8-Methoxy-11-oxo-5-(toluene-4-sulfonyl)-6,11-dihydro-5H-dibenzo[b,e]azepine-3-carbonyl chloride

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Technology Process of 8-Methoxy-11-oxo-5-(toluene-4-sulfonyl)-6,11-dihydro-5H-dibenzo[b,e]azepine-3-carbonyl chloride

There total 5 articles about 8-Methoxy-11-oxo-5-(toluene-4-sulfonyl)-6,11-dihydro-5H-dibenzo[b,e]azepine-3-carbonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 78382-92-0
2-[(3-Methoxy-benzyl)-(toluene-4-sulfonyl)-amino]-terephthaloyl dichloride

: 78382-93-1
8-Methoxy-11-oxo-5-(toluene-4-sulfonyl)-6,11-dihydro-5H-dibenzo[b,e]azepine-3-carbonyl chloride

: 8-Methoxy-11-oxo-5-(toluene-4-sulfonyl)-6,11-dihydro-5H-dibenzo[b,e]azepine-3-carboxylic acid

Guidance literature:: With tin(IV) chloride; In benzene; for 18h;
DOI:10.1021/jm00141a018

Reference yield:

: 68218-51-9
N-(p-toluenesulphonyl)-2,5-dimethoxycarbonylanilide

: 78382-93-1
8-Methoxy-11-oxo-5-(toluene-4-sulfonyl)-6,11-dihydro-5H-dibenzo[b,e]azepine-3-carbonyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) sodium hydride / 1.) DMF, 2.) DMF, 16 h

2: aq. methanolic sodium hydroxide / 3 h / Heating

3: thionyl chloride / Heating

4: 60 percent / SnCl₄ / benzene / 18 h

With sodium hydroxide; thionyl chloride; tin(IV) chloride; sodium hydride; In benzene;
DOI:10.1021/jm00141a018

Reference yield:

: 344270-34-4
2-[(3-Methoxy-benzyl)-(toluene-4-sulfonyl)-amino]-terephthalic acid

: 78382-93-1
8-Methoxy-11-oxo-5-(toluene-4-sulfonyl)-6,11-dihydro-5H-dibenzo[b,e]azepine-3-carbonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / Heating

2: 60 percent / SnCl₄ / benzene / 18 h

With thionyl chloride; tin(IV) chloride; In benzene;
DOI:10.1021/jm00141a018