2-[(3-Methoxy-benzyl)-(toluene-4-sulfonyl)-amino]-terephthaloyl dichloride

Base Information

Chemical Name:2-[(3-Methoxy-benzyl)-(toluene-4-sulfonyl)-amino]-terephthaloyl dichloride
CAS No.:78382-92-0
Molecular Formula:C₂₃H₁₉Cl₂NO₅S
Molecular Weight:492.38
Hs Code.:

Synonyms:2-[(3-Methoxy-benzyl)-(toluene-4-sulfonyl)-amino]-terephthaloyl dichloride

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Chemical Property of 2-[(3-Methoxy-benzyl)-(toluene-4-sulfonyl)-amino]-terephthaloyl dichloride

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Technology Process of 2-[(3-Methoxy-benzyl)-(toluene-4-sulfonyl)-amino]-terephthaloyl dichloride

There total 5 articles about 2-[(3-Methoxy-benzyl)-(toluene-4-sulfonyl)-amino]-terephthaloyl dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 78382-92-0
2-[(3-Methoxy-benzyl)-(toluene-4-sulfonyl)-amino]-terephthaloyl dichloride

Guidance literature:: Multi-step reaction with 4 steps

1: 60 percent / pyridine / 24 h / Ambient temperature

2: 1.) sodium hydride / 1.) DMF, 2.) DMF, 16 h

3: aq. methanolic sodium hydroxide / 3 h / Heating

4: thionyl chloride / Heating

With sodium hydroxide; thionyl chloride; sodium hydride; In pyridine;
DOI:10.1021/jm00141a018

Reference yield:

: 344270-34-4
2-[(3-Methoxy-benzyl)-(toluene-4-sulfonyl)-amino]-terephthalic acid

: 78382-92-0
2-[(3-Methoxy-benzyl)-(toluene-4-sulfonyl)-amino]-terephthaloyl dichloride

Guidance literature:: With thionyl chloride; Yield given; Heating;
DOI:10.1021/jm00141a018

Reference yield:

: 68218-51-9
N-(p-toluenesulphonyl)-2,5-dimethoxycarbonylanilide

: 78382-92-0
2-[(3-Methoxy-benzyl)-(toluene-4-sulfonyl)-amino]-terephthaloyl dichloride

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium hydride / 1.) DMF, 2.) DMF, 16 h

2: aq. methanolic sodium hydroxide / 3 h / Heating

3: thionyl chloride / Heating

With sodium hydroxide; thionyl chloride; sodium hydride;
DOI:10.1021/jm00141a018