*,R^*)>-methyl α-methoxy-β-<(3-methoxy-3-oxopropyl)thio>-2-(8-phenyloctyl)benzenepropanoate

Base Information

• Chemical Name: *,R^*)>-methyl α-methoxy-β-<(3-methoxy-3-oxopropyl)thio>-2-(8-phenyloctyl)benzenepropanoate
• CAS No.: 121441-87-0
• Molecular Formula: C₂₉H₄₀O₅S
• Molecular Weight: 500.7

Synonyms:*,R^*)>-methyl α-methoxy-β-<(3-methoxy-3-oxopropyl)thio>-2-(8-phenyloctyl)benzenepropanoate

Chemical Property of *,R^*)>-methyl α-methoxy-β-<(3-methoxy-3-oxopropyl)thio>-2-(8-phenyloctyl)benzenepropanoate

Chemical Property:

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Technology Process of *,R^*)>-methyl α-methoxy-β-<(3-methoxy-3-oxopropyl)thio>-2-(8-phenyloctyl)benzenepropanoate

There total 2 articles about *,R^*)>-methyl α-methoxy-β-<(3-methoxy-3-oxopropyl)thio>-2-(8-phenyloctyl)benzenepropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

methanol (67-56-1) + <4R-<3(2S*,3S*),4α,5α>>-methyl 2-<<2-methoxy-3-(4-methyl-2-oxo-5-phenyl-3-oxazolidinyl)-3-oxo-1-<2-(8-phenyloctyl)phenyl>propyl>thio>propanoate (121441-86-9) → *,R*)>-methyl α-methoxy-β-<(3-methoxy-3-oxopropyl)thio>-2-(8-phenyloctyl)benzenepropanoate (121441-87-0)

Guidance literature:

With sodium methylate; at 0 ℃; for 0.333333h;

DOI:10.1021/jo00275a045

Reference yield:

Methyl 3-mercaptopropionate (2935-90-2) + Methyl 2-methoxy-3-hydroxy-3-[2-(8-phenyloctyl)phenyl ]propanoate (121441-81-4,121521-50-4,121521-51-5) → methyl 2-methoxy-3-(2-carbomethoxyethylthio)-3-[2-(8-phenyloctyl)phenyl]propanoate (121441-84-7,121441-87-0,121521-54-8,121569-38-8)

Guidance literature:

With trifluoroacetic acid; for 18h; Yield given; Ambient temperature;

DOI:10.1021/jo00275a045

Reference yield: 69.0%

*,R*)>-methyl α-methoxy-β-<(3-methoxy-3-oxopropyl)thio>-2-(8-phenyloctyl)benzenepropanoate (121441-87-0) → *,R*)>-β-<(2-carboxyethyl)thio>-α-methoxy-2-(8-phenyloctyl)benzenepropanoic acid (121441-88-1)

Guidance literature:

With sodium hydroxide; In methanol; for 18h;

DOI:10.1021/jo00275a045

upstream raw materials:

Methyl 3-mercaptopropionate

Methyl 2-methoxy-3-hydroxy-3-[2-(8-phenyloctyl)phenyl ]propanoate

methanol

<4R-<3(2S^*,3S^*),4α,5α>>-methyl 2-<<2-methoxy-3-(4-methyl-2-oxo-5-phenyl-3-oxazolidinyl)-3-oxo-1-<2-(8-phenyloctyl)phenyl>propyl>thio>propanoate

Downstream raw materials:

(R^*,S^*)-β-<(2-carboxyethyl)thio>-α-methoxy-2-(8-phenyloctyl)benzenepropanoic acid

(R^*,R^*)-β-<(2-carboxyethyl)thio>-α-methoxy-2-(8-phenyloctyl)benzenepropanoic acid

*,R^*)>-β-<(2-carboxyethyl)thio>-α-methoxy-2-(8-phenyloctyl)benzenepropanoic acid

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