Technology Process of C22H28N2O4
There total 1 articles about C22H28N2O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
(2R)-(tert-butoxycarbonylamino)-4-phenylbutanoic acid;
With
benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
at 22 ℃;
for 0.25h;
O-benzylhydoxylamine hydrochloride;
In
N,N-dimethyl-formamide;
for 0.5h;
- Guidance literature:
-
C22H28N2O4;
With
hydrogenchloride; triethylsilane;
In
1,4-dioxane;
at 22 ℃;
for 12.5h;
With
sodium hydroxide;
In
1,4-dioxane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogenchloride; triethylsilane / 1,4-dioxane / 12.5 h / 22 °C
2.1: sodium cyanoborohydride / methanol / 1 h / 0 °C
2.2: 4 h
3.1: hydrogenchloride / 1,4-dioxane; diethyl ether / 22 °C
4.1: diethylamine / trisodium tris(3-sulfophenyl)phosphine; palladium diacetate / acetonitrile; water / 0.25 h / 22 °C
With
hydrogenchloride; triethylsilane; sodium cyanoborohydride; diethylamine;
trisodium tris(3-sulfophenyl)phosphine; palladium diacetate;
In
1,4-dioxane; methanol; diethyl ether; water; acetonitrile;