(2R)-4-phenyl-N-(phenylmethoxy)-2-[({4-[(prop-2-enyloxycarbonylamino)methyl]phenyl}methyl)amino]butanamide hydrochloride

Base Information

Chemical Name:(2R)-4-phenyl-N-(phenylmethoxy)-2-[({4-[(prop-2-enyloxycarbonylamino)methyl]phenyl}methyl)amino]butanamide hydrochloride
CAS No.:1173158-88-7
Molecular Formula:C₂₉H₃₃N₃O₄*ClH
Molecular Weight:524.06
Hs Code.:

Synonyms:(2R)-4-phenyl-N-(phenylmethoxy)-2-[({4-[(prop-2-enyloxycarbonylamino)methyl]phenyl}methyl)amino]butanamide hydrochloride

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Chemical Property of (2R)-4-phenyl-N-(phenylmethoxy)-2-[({4-[(prop-2-enyloxycarbonylamino)methyl]phenyl}methyl)amino]butanamide hydrochloride

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Technology Process of (2R)-4-phenyl-N-(phenylmethoxy)-2-[({4-[(prop-2-enyloxycarbonylamino)methyl]phenyl}methyl)amino]butanamide hydrochloride

There total 9 articles about (2R)-4-phenyl-N-(phenylmethoxy)-2-[({4-[(prop-2-enyloxycarbonylamino)methyl]phenyl}methyl)amino]butanamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1173238-91-9
(2R)-4-phenyl-N-(phenylmethoxy)-2-[({4-[(prop-2-enyloxycarbonylamino)methyl]phenyl}methyl)amino]butanamide

: 1173158-88-7
(2R)-4-phenyl-N-(phenylmethoxy)-2-[({4-[(prop-2-enyloxycarbonylamino)methyl]phenyl}methyl)amino]butanamide hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; diethyl ether; at 22 ℃;

Reference yield:

: 1173158-87-6
C₂₂H₂₈N₂O₄

: 1173158-88-7
(2R)-4-phenyl-N-(phenylmethoxy)-2-[({4-[(prop-2-enyloxycarbonylamino)methyl]phenyl}methyl)amino]butanamide hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; triethylsilane / 1,4-dioxane / 12.5 h / 22 °C

2.1: sodium cyanoborohydride / methanol / 1 h / 0 °C

2.2: 4 h

3.1: hydrogenchloride / 1,4-dioxane; diethyl ether / 22 °C

With hydrogenchloride; triethylsilane; sodium cyanoborohydride; In 1,4-dioxane; methanol; diethyl ether;

Reference yield:

: 6232-11-7
methyl 4-(aminomethyl)benzoate hydrochloride

: 1173158-88-7
(2R)-4-phenyl-N-(phenylmethoxy)-2-[({4-[(prop-2-enyloxycarbonylamino)methyl]phenyl}methyl)amino]butanamide hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h / 0 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C

2.2: 0.25 h

3.1: Dess-Martin periodane / dichloromethane / 0.08 h / 22 °C / Reflux

4.1: sodium cyanoborohydride / methanol / 1 h / 0 °C

4.2: 4 h

5.1: hydrogenchloride / 1,4-dioxane; diethyl ether / 22 °C

With hydrogenchloride; lithium aluminium tetrahydride; sodium cyanoborohydride; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; dichloromethane;