methyl (2S,3R,5S)-5-(tert-butyldimethylsilyloxy)-2-(tert butyldiphenylsilyloxy)-3-hydroxy-7-[methoxy(methyl)amino]-7-oxoheptanoate

Base Information

Chemical Name:methyl (2S,3R,5S)-5-(tert-butyldimethylsilyloxy)-2-(tert butyldiphenylsilyloxy)-3-hydroxy-7-[methoxy(methyl)amino]-7-oxoheptanoate
CAS No.:1240466-94-7
Molecular Formula:C₃₂H₅₁NO₇Si₂
Molecular Weight:617.93
Hs Code.:

Synonyms:methyl (2S,3R,5S)-5-(tert-butyldimethylsilyloxy)-2-(tert butyldiphenylsilyloxy)-3-hydroxy-7-[methoxy(methyl)amino]-7-oxoheptanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (2S,3R,5S)-5-(tert-butyldimethylsilyloxy)-2-(tert butyldiphenylsilyloxy)-3-hydroxy-7-[methoxy(methyl)amino]-7-oxoheptanoate

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Technology Process of methyl (2S,3R,5S)-5-(tert-butyldimethylsilyloxy)-2-(tert butyldiphenylsilyloxy)-3-hydroxy-7-[methoxy(methyl)amino]-7-oxoheptanoate

There total 1 articles about methyl (2S,3R,5S)-5-(tert-butyldimethylsilyloxy)-2-(tert butyldiphenylsilyloxy)-3-hydroxy-7-[methoxy(methyl)amino]-7-oxoheptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1240466-93-6
methyl (S)-2-[(2R,4S)-4-(tert-butyldimethylsilyloxy)-6-oxotetrahydro-2H-pyran-2-yl]-2-(tert-butyldiphenylsilyloxy)acetate

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 1240466-94-7
methyl (2S,3R,5S)-5-(tert-butyldimethylsilyloxy)-2-(tert butyldiphenylsilyloxy)-3-hydroxy-7-[methoxy(methyl)amino]-7-oxoheptanoate

Guidance literature:: N,O-dimethylhydroxylamine*hydrochloride; With trimethylaluminum; In hexane; dichloromethane; at -78 - 20 ℃; Inert atmosphere;

methyl (S)-2-[(2R,4S)-4-(tert-butyldimethylsilyloxy)-6-oxotetrahydro-2H-pyran-2-yl]-2-(tert-butyldiphenylsilyloxy)acetate; In hexane; dichloromethane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1002/ejoc.201000369

Reference yield: 85.0%

: 1240466-94-7
methyl (2S,3R,5S)-5-(tert-butyldimethylsilyloxy)-2-(tert butyldiphenylsilyloxy)-3-hydroxy-7-[methoxy(methyl)amino]-7-oxoheptanoate

: 420-37-1
trimethoxonium tetrafluoroborate

: 1240466-95-8
methyl (2S,3R,5S)-5-(tert-butyldimethylsilyloxy)-2-(tert butyldiphenylsilyloxy)-3-methoxy-7-[methoxy(methyl)amino]-7-oxoheptanoate

Guidance literature:: With N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; In dichloromethane; at -5 ℃; for 6h; Inert atmosphere;
DOI:10.1002/ejoc.201000369