methyl (2,5-dihydrophenyl)acetic acid

Base Information

• Chemical Name: methyl (2,5-dihydrophenyl)acetic acid
• CAS No.: 75996-10-0
• Molecular Formula: C₉H₁₂O₂
• Molecular Weight: 152.193
• Mol file: 75996-10-0.mol

Synonyms:methyl (2,5-dihydrophenyl)acetic acid

Chemical Property of methyl (2,5-dihydrophenyl)acetic acid

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of methyl (2,5-dihydrophenyl)acetic acid

There total 1 articles about methyl (2,5-dihydrophenyl)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

methanol (67-56-1) + 2-(cyclohexa-1,4-dien-1-yl)acetic acid (27008-28-2) → methyl (2,5-dihydrophenyl)acetic acid (75996-10-0)

Guidance literature:

With acetyl chloride; for 6h; Heating;

DOI:10.1021/jo00319a029

Reference yield: 84.0%

methyl (2,5-dihydrophenyl)acetic acid (75996-10-0) → 1-<(carbomethoxy)methyl>-trans-4,5-dibromo-1-cyclohexene (76251-09-7)

Guidance literature:

With bromine; In tetrachloromethane; at 0 ℃;

DOI:10.1021/jo00319a029

Reference yield: 73.0%

methyl (2,5-dihydrophenyl)acetic acid (75996-10-0) → benzeneacetic acid methyl ester (101-41-7)

Guidance literature:

With manganese(IV) oxide; In methyl cyclohexane; at 70 ℃; for 18h;

DOI:10.1021/ja983041s

upstream raw materials:

methanol

2-(cyclohexa-1,4-dien-1-yl)acetic acid

Downstream raw materials:

1-<(carbomethoxy)methyl>-trans-4,5-dibromo-1-cyclohexene

benzeneacetic acid methyl ester