[PtMe(N,N'-bis(2,6-diisopropylphenyl)butane-2,3-diimine)(propylene)]BF₄

Base Information

Chemical Name:[PtMe(N,N'-bis(2,6-diisopropylphenyl)butane-2,3-diimine)(propylene)]BF₄
CAS No.:199284-76-9
Molecular Formula:BF₄*C₃₂H₄₉N₂Pt
Molecular Weight:743.639
Hs Code.:

[PtMe(N,N'-bis(2,6-diisopropylphenyl)butane-2,3-diimine)(propylene)]BF<sub>4</sub>

Synonyms:[PtMe(N,N'-bis(2,6-diisopropylphenyl)butane-2,3-diimine)(propylene)]BF₄

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Chemical Property of [PtMe(N,N'-bis(2,6-diisopropylphenyl)butane-2,3-diimine)(propylene)]BF₄

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Technology Process of [PtMe(N,N'-bis(2,6-diisopropylphenyl)butane-2,3-diimine)(propylene)]BF₄

There total 2 articles about [PtMe(N,N'-bis(2,6-diisopropylphenyl)butane-2,3-diimine)(propylene)]BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 14104-20-2
silver tetrafluoroborate

: 187737-37-7,13987-01-4,15220-87-8,9003-07-0,676-63-1,25085-53-4
propene

: 199284-91-8
[PtCl(Me)(diacetyl bis(2,6-diisopropylphenylimine))]

: 199284-76-9
[Pt(Me)(diacetyl bis(2,6-diisopropylphenylimine))(propylene)](BF₄)

Guidance literature:: In dichloromethane; byproducts: AgCl; mixing AgBF4 and excess of propylene, addn. of Pt-complex at 273 K, stirring for 48 h at room temp.; filtration off of AgCl (Celite), concn., crystn. on addn. of MePh and standing at 277 K, washing (MePh, pentane), drying (vac.); NMR spectroscopy;
DOI:10.1021/om970428f

Reference yield:

: 1,4-di(2,6-diisopropylphenyl)-2,3-dimethyl-1,4-diazabutadiene

: 199284-76-9
[Pt(Me)(diacetyl bis(2,6-diisopropylphenylimine))(propylene)](BF₄)

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether

2: dichloromethane

In diethyl ether; dichloromethane;
DOI:10.1021/om970428f

Reference yield: 70.0%

: 199284-76-9
[PtMe(N,N'-bis(2,6-diisopropylphenyl)butane-2,3-diimine)(propylene)]BF₄

: 691894-17-4
[PtMe(N,N'-(1,2-dimethyl-1,2-ethanediylidene)bis(2,6-diisopropylaniline)))(propylene)]

Guidance literature:: With KOH; In methanol; soln. of KOH in methanol was added to stirred suspn. of Pt complex in methanol kept in ice bath; mixt. was stirred for 15 min; septd.; washed (cold methanol); dried (vac.); elem. anal.;
DOI:10.1021/om049968k