(Z)-N-methoxy-4-methylcarbamoylbenzenecarboximidoyl bromide

Base Information

Chemical Name:(Z)-N-methoxy-4-methylcarbamoylbenzenecarboximidoyl bromide
CAS No.:260430-05-5
Molecular Formula:C₁₀H₁₁BrN₂O₂
Molecular Weight:271.114
Hs Code.:

Synonyms:(Z)-N-methoxy-4-methylcarbamoylbenzenecarboximidoyl bromide

Suppliers and Price of (Z)-N-methoxy-4-methylcarbamoylbenzenecarboximidoyl bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-N-methoxy-4-methylcarbamoylbenzenecarboximidoyl bromide

Chemical Property:

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Technology Process of (Z)-N-methoxy-4-methylcarbamoylbenzenecarboximidoyl bromide

There total 4 articles about (Z)-N-methoxy-4-methylcarbamoylbenzenecarboximidoyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: C₉H₇BrClNO₂

: 74-89-5
methylamine

: 260430-05-5
(Z)-N-methoxy-4-methylcarbamoylbenzenecarboximidoyl bromide

Guidance literature:: In water; benzene;
DOI:10.1080/00397919308018582

Reference yield:

: 1679-64-7
Monomethyl terephthalate

: 260430-05-5
(Z)-N-methoxy-4-methylcarbamoylbenzenecarboximidoyl bromide

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / Et₃N, PPh₃-CBr₄ / acetonitrile / 3 h / Heating

2: 89 percent / 10percent aq. HBr / dioxane / 11 h / Heating

3: SOCl₂ / 2 h / Heating

4: 84 percent / H₂O; benzene

With thionyl chloride; carbon tetrabromide; hydrogen bromide; triethylamine; triphenylphosphine; In 1,4-dioxane; water; acetonitrile; benzene;
DOI:10.1080/00397919308018582

Reference yield:

: 137042-68-3
C₁₀H₁₀BrNO₃

: 260430-05-5
(Z)-N-methoxy-4-methylcarbamoylbenzenecarboximidoyl bromide

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / 10percent aq. HBr / dioxane / 11 h / Heating

2: SOCl₂ / 2 h / Heating

3: 84 percent / H₂O; benzene

With thionyl chloride; hydrogen bromide; In 1,4-dioxane; water; benzene;
DOI:10.1080/00397919308018582