triethylammonium 3,4-bis(benzyloxy)-5-(ethoxycarbonyl)-1-(4-methoxyphenyl)-1H-pyrrole-2-carboxylate

Base Information

Chemical Name:triethylammonium 3,4-bis(benzyloxy)-5-(ethoxycarbonyl)-1-(4-methoxyphenyl)-1H-pyrrole-2-carboxylate
CAS No.:1443053-94-8
Molecular Formula:C₆H₁₅N*C₂₉H₂₇NO₇
Molecular Weight:602.728
Hs Code.:

Synonyms:triethylammonium 3,4-bis(benzyloxy)-5-(ethoxycarbonyl)-1-(4-methoxyphenyl)-1H-pyrrole-2-carboxylate

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Chemical Property of triethylammonium 3,4-bis(benzyloxy)-5-(ethoxycarbonyl)-1-(4-methoxyphenyl)-1H-pyrrole-2-carboxylate

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Technology Process of triethylammonium 3,4-bis(benzyloxy)-5-(ethoxycarbonyl)-1-(4-methoxyphenyl)-1H-pyrrole-2-carboxylate

There total 4 articles about triethylammonium 3,4-bis(benzyloxy)-5-(ethoxycarbonyl)-1-(4-methoxyphenyl)-1H-pyrrole-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1443053-92-6
diethyl 3,4-bis(benzyloxy)-1-(4-methoxyphenyl)-1H-pyrrole-2,5-dicarboxylate

: 121-44-8
triethylamine

: 1443053-94-8
triethylammonium 3,4-bis(benzyloxy)-5-(ethoxycarbonyl)-1-(4-methoxyphenyl)-1H-pyrrole-2-carboxylate

Guidance literature:: diethyl 3,4-bis(benzyloxy)-1-(4-methoxyphenyl)-1H-pyrrole-2,5-dicarboxylate; With water; sodium hydroxide; In tetrahydrofuran; ethanol; at 50 ℃; for 16h;

triethylamine; In tetrahydrofuran; ethanol; water;

Reference yield:

: 104-94-9
4-methoxy-aniline

: 1443053-94-8
triethylammonium 3,4-bis(benzyloxy)-5-(ethoxycarbonyl)-1-(4-methoxyphenyl)-1H-pyrrole-2-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: N-ethyl-N,N-diisopropylamine / acetonitrile / 16 h / 60 °C

2: sodium ethanolate / ethanol / 1 h / 100 °C

3: potassium carbonate / N,N-dimethyl-formamide / 4 h / 60 °C

4: sodium hydroxide; water / tetrahydrofuran; ethanol / 16 h / 50 °C

With water; sodium ethanolate; potassium carbonate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 98269-30-8
diethyl 2,2’-((4-methoxyphenyl)azanediyl)diacetate

: 1443053-94-8
triethylammonium 3,4-bis(benzyloxy)-5-(ethoxycarbonyl)-1-(4-methoxyphenyl)-1H-pyrrole-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium ethanolate / ethanol / 1 h / 100 °C

2: potassium carbonate / N,N-dimethyl-formamide / 4 h / 60 °C

3: sodium hydroxide; water / tetrahydrofuran; ethanol / 16 h / 50 °C

With water; sodium ethanolate; potassium carbonate; sodium hydroxide; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;