C₃₉H₃₇ClN₂O₅

Base Information

Chemical Name:C₃₉H₃₇ClN₂O₅
CAS No.:1354189-98-2
Molecular Formula:C₃₉H₃₇ClN₂O₅
Molecular Weight:649.186
Hs Code.:

C<sub>39</sub>H<sub>37</sub>ClN<sub>2</sub>O<sub>5</sub>

Synonyms:C₃₉H₃₇ClN₂O₅

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Chemical Property of C₃₉H₃₇ClN₂O₅

Chemical Property:

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Technology Process of C₃₉H₃₇ClN₂O₅

There total 18 articles about C₃₉H₃₇ClN₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1354189-97-1
(S)-(9H-fluoren-9-yl)methyl 2-(6-(1-tert-butoxy-2-hydroxyethyl)-5-(4-chlorophenyl)-7-methyl-2-oxoquinolin-1(2H)-yl)ethylcarbamate

: 1354189-98-2
C₃₉H₃₇ClN₂O₅

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 1.5h;

Reference yield:

: 50741-92-9
2-methyl-4-nitroanisole

: 1354189-98-2
C₃₉H₃₇ClN₂O₅

Guidance literature:: Multi-step reaction with 17 steps

1.1: tin(II) chloride dihdyrate / triphenylphosphine; rhodium(III) chloride hydrate / isopropyl alcohol; 1,4-dioxane; water / 20 h / 180 °C / Inert atmosphere

2.1: N-Bromosuccinimide; sulfuric acid / 3.5 h / 15 °C

2.2: pH 10 / Cooling with ice

3.1: boron tribromide / dichloromethane / 3 h

3.2: 0.33 h / 0 °C

4.1: pyridine / dichloromethane / 2 h / -30 - 0 °C

5.1: lithium chloride / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide; 1,4-dioxane / 16 h / 80 °C / Inert atmosphere

6.1: hydroquinine 1,4-phthalazinediyl diether / water; tert-butyl alcohol / 48 h / 0 °C

7.1: pyridine / dichloromethane / 12 h / 0 - 20 °C

8.1: perchloric acid / 2 h / 25 °C

9.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 12 h

10.1: 10 h / 140 °C

11.1: methylamine / ethanol; water / 1.33 h / 78 °C

12.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 1.5 h / 100 °C

13.1: sodium hydroxide; methanol / tetrahydrofuran / 16 h / 25 °C

14.1: 1H-imidazole / N,N-dimethyl-formamide / 0 - 20 °C

15.1: potassium tert-butylate / N,N-dimethyl-formamide / 0.5 h

15.2: 20 °C

16.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

16.2: 0 - 20 °C

17.1: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C

With pyridine; 1H-imidazole; methanol; N-Bromosuccinimide; perchloric acid; tin(II) chloride dihdyrate; hydroquinine 1,4-phthalazinediyl diether; sulfuric acid; potassium tert-butylate; tetrabutyl ammonium fluoride; boron tribromide; potassium carbonate; Dess-Martin periodane; 3-chloro-benzenecarboperoxoic acid; methylamine; lithium chloride; sodium hydroxide; bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; rhodium(III) chloride hydrate; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol; tert-butyl alcohol;

Reference yield:

: 467219-83-6
6-methoxy-7-methylquinoline

: 1354189-98-2
C₃₉H₃₇ClN₂O₅

Guidance literature:: Multi-step reaction with 16 steps

1.1: N-Bromosuccinimide; sulfuric acid / 3.5 h / 15 °C

1.2: pH 10 / Cooling with ice

2.1: boron tribromide / dichloromethane / 3 h

2.2: 0.33 h / 0 °C

3.1: pyridine / dichloromethane / 2 h / -30 - 0 °C

4.1: lithium chloride / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide; 1,4-dioxane / 16 h / 80 °C / Inert atmosphere

5.1: hydroquinine 1,4-phthalazinediyl diether / water; tert-butyl alcohol / 48 h / 0 °C

6.1: pyridine / dichloromethane / 12 h / 0 - 20 °C

7.1: perchloric acid / 2 h / 25 °C

8.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 12 h

9.1: 10 h / 140 °C

10.1: methylamine / ethanol; water / 1.33 h / 78 °C

11.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 1.5 h / 100 °C

12.1: sodium hydroxide; methanol / tetrahydrofuran / 16 h / 25 °C

13.1: 1H-imidazole / N,N-dimethyl-formamide / 0 - 20 °C

14.1: potassium tert-butylate / N,N-dimethyl-formamide / 0.5 h

14.2: 20 °C

15.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

15.2: 0 - 20 °C

16.1: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C

With pyridine; 1H-imidazole; methanol; N-Bromosuccinimide; perchloric acid; hydroquinine 1,4-phthalazinediyl diether; sulfuric acid; potassium tert-butylate; tetrabutyl ammonium fluoride; boron tribromide; potassium carbonate; Dess-Martin periodane; 3-chloro-benzenecarboperoxoic acid; methylamine; lithium chloride; sodium hydroxide; bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;