(R,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-4,4-dimethylpent-2-en-1-ol

Base Information

Chemical Name:(R,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-4,4-dimethylpent-2-en-1-ol
CAS No.:868744-82-5
Molecular Formula:C₁₇H₃₂O
Molecular Weight:252.44
Hs Code.:

Synonyms:(R,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-4,4-dimethylpent-2-en-1-ol

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Chemical Property of (R,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-4,4-dimethylpent-2-en-1-ol

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Technology Process of (R,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-4,4-dimethylpent-2-en-1-ol

There total 1 articles about (R,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-4,4-dimethylpent-2-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61382-45-4
(E)-1-iodo-3,3-dimethyl-1-butene

: 80434-59-9,485843-44-5,796865-68-4
(1R,2S,5R)-2-isopropyl-5-methylcyclohexanecarboxaldehyde

: 868744-82-5
(R,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-4,4-dimethylpent-2-en-1-ol

Guidance literature:: (E)-1-iodo-3,3-dimethyl-1-butene; With tert.-butyl lithium; In diethyl ether; pentane; at -78 - 20 ℃; for 2.5h;

(1R,2S,5R)-2-isopropyl-5-methylcyclohexanecarboxaldehyde; With trimethylaluminum; In diethyl ether; hexane; pentane; at -78 ℃; for 3h;
DOI:10.1021/ol052034n

Reference yield: 99.0%

: 868744-82-5
(R,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-4,4-dimethylpent-2-en-1-ol

: (1S,2S,4R)-2-((E)-3-Azido-4,4-dimethyl-pent-1-enyl)-1-isopropyl-4-methyl-cyclohexane

Guidance literature:: With tris-(2-chloro-ethyl)-amine; diethylazodicarboxylate; In benzene; at 0 - 20 ℃;
DOI:10.1021/jo800817p

Reference yield: 99.0%

: 868744-82-5
(R,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-4,4-dimethylpent-2-en-1-ol

: 75-15-0,12122-00-8
carbon disulfide

: 74-88-4
methyl iodide

: C₁₉H₃₄OS₂

Guidance literature:: (R,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-4,4-dimethylpent-2-en-1-ol; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 1h;

carbon disulfide; In tetrahydrofuran; for 2h; Heating;

methyl iodide; In tetrahydrofuran; for 0.75h; Further stages.; Heating;
DOI:10.1139/V07-091