3-ethylthiophthalic acid

Base Information

Chemical Name:3-ethylthiophthalic acid
CAS No.:18245-63-1
Molecular Formula:C₁₀H₁₀O₄S
Molecular Weight:226.253
Hs Code.:

Synonyms:3-ethylthiophthalic acid

Suppliers and Price of 3-ethylthiophthalic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-ethylthiophthalic acid

Chemical Property:

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Technology Process of 3-ethylthiophthalic acid

There total 4 articles about 3-ethylthiophthalic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1207091-08-4
3-ethylthio-N-phenylphthalimide

: 18245-63-1
3-ethylthiophthalic acid

Guidance literature:: 3-ethylthio-N-phenylphthalimide; With water; sodium hydroxide; at 145 ℃; for 6h; autoclave;

With hydrogenchloride; In water;

Reference yield:

: 117-21-5
3-chlorophthalic anhydride

: 18245-63-1
3-ethylthiophthalic acid

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid / 3 h / Reflux

2: sodium hydrosulfide monohydrate / water; N,N-dimethyl-formamide / 6 h / 85 °C / Inert atmosphere

3: potassium carbonate / acetonitrile / 3 h / Reflux

4: water; sodium hydroxide / 6 h / 145 °C / autoclave

With sodium hydrosulfide monohydrate; water; potassium carbonate; sodium hydroxide; In water; acetic acid; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 42899-83-2
3-chloro-N-phenylphthalimide

: 18245-63-1
3-ethylthiophthalic acid

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrosulfide monohydrate / water; N,N-dimethyl-formamide / 6 h / 85 °C / Inert atmosphere

2: potassium carbonate / acetonitrile / 3 h / Reflux

3: water; sodium hydroxide / 6 h / 145 °C / autoclave

With sodium hydrosulfide monohydrate; water; potassium carbonate; sodium hydroxide; In water; N,N-dimethyl-formamide; acetonitrile;