naphth-1-yl-glycine benzyl ester phosphorochloridate

Base Information

Chemical Name:naphth-1-yl-glycine benzyl ester phosphorochloridate
CAS No.:1228377-60-3
Molecular Formula:C₁₉H₁₇ClNO₄P
Molecular Weight:389.775
Hs Code.:

Synonyms:naphth-1-yl-glycine benzyl ester phosphorochloridate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of naphth-1-yl-glycine benzyl ester phosphorochloridate

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Technology Process of naphth-1-yl-glycine benzyl ester phosphorochloridate

There total 2 articles about naphth-1-yl-glycine benzyl ester phosphorochloridate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 31651-76-0
1-naphthyl dichlorophosphate

: 2462-31-9
benzyl 2-aminoacetate hydrochloride

: 1228377-60-3
naphth-1-yl-glycine benzyl ester phosphorochloridate

Guidance literature:: With triethylamine; In dichloromethane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmc.2010.02.015

Reference yield:

: 31651-76-0
1-naphthyl dichlorophosphate

: 1228377-60-3
naphth-1-yl-glycine benzyl ester phosphorochloridate

Guidance literature:: With triethylamine; In dichloromethane; at -78 ℃;
DOI:10.1016/j.bmcl.2016.10.077

Reference yield: 7.8%

: 1228377-60-3
naphth-1-yl-glycine benzyl ester phosphorochloridate

: 69304-47-8
(E)-5-(2-bromovinyl)-2'-deoxyuridine

: (E)-5-(2-bromovinyl)-2’-deoxyuridine-5’-[1-naphthyl(benzyloxyglycinyl)]phosphate

Guidance literature:: With 1-methyl-1H-imidazole; In tetrahydrofuran; at -78 - 20 ℃; for 12.5167h; Inert atmosphere;
DOI:10.1016/j.bmcl.2016.10.077