2-(chlorocarbonyl)-1-Fmoc-2-benzylhydrazine

Base Information

Chemical Name:2-(chlorocarbonyl)-1-Fmoc-2-benzylhydrazine
CAS No.:861851-74-3
Molecular Formula:C₂₃H₁₉ClN₂O₃
Molecular Weight:406.868
Hs Code.:

Synonyms:2-(chlorocarbonyl)-1-Fmoc-2-benzylhydrazine

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Chemical Property of 2-(chlorocarbonyl)-1-Fmoc-2-benzylhydrazine

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Technology Process of 2-(chlorocarbonyl)-1-Fmoc-2-benzylhydrazine

There total 5 articles about 2-(chlorocarbonyl)-1-Fmoc-2-benzylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₆H₂₆N₂O₃S

: 861851-74-3
2-(chlorocarbonyl)-1-Fmoc-2-benzylhydrazine

Guidance literature:: C₂₆H₂₆N₂O₃S; With tetrabutyl-ammonium chloride; In acetonitrile; at 20 ℃; for 0.0166667h;

With trichloroisocyanuric acid; In acetonitrile; at 20 ℃; for 0.0833333h;

Reference yield:

: 147688-35-5
C₂₇H₂₈N₂O₄

: 861851-74-3
2-(chlorocarbonyl)-1-Fmoc-2-benzylhydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.6 g / CF₃CO₂H / H₂O / 2 h / 20 °C

2: tetrahydrofuran; toluene / 16 h / 20 °C

With trifluoroacetic acid; In tetrahydrofuran; water; toluene;
DOI:10.1016/j.bmc.2005.04.048

Reference yield:

: 35661-51-9
N-(9-fluorenylmethyloxycarbonyl)hydrazine

: 861851-74-3
2-(chlorocarbonyl)-1-Fmoc-2-benzylhydrazine

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / 2 h / Reflux

2: 20 % Pd(OH)2/C; hydrogen / tetrahydrofuran / 14 h / 20 °C / 5171.62 Torr

3: dichloromethane; toluene / 0.08 h / 0 °C / Inert atmosphere

With 20 % Pd(OH)2/C; hydrogen; In tetrahydrofuran; ethanol; dichloromethane; toluene;
DOI:10.1021/jo300311q