Technology Process of 6-(10-acetoxydecyl)-2,3-dimethoxy-5-methylphenol
There total 8 articles about 6-(10-acetoxydecyl)-2,3-dimethoxy-5-methylphenol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
2: 95 percent / dimethylsulfoxide / 15 h / 80 °C
3: 86 percent / NaOH, 3N HCl / ethanol / 19 h / Heating
4: PCl5 / CH2Cl2 / 2 h / 25 °C
5: 44 percent / AlCl3 / 1,2-dichloro-ethane / 72 h / 20 °C
6: 79 percent / NaOH / methanol / 2 h / Ambient temperature
7: H2, 70percent HClO4 / 5percent Pd-C / 24 h / Ambient temperature
With
hydrogenchloride; sodium hydroxide; aluminium trichloride; perchloric acid; phosphorus pentachloride; hydrogen;
palladium on activated charcoal;
In
methanol; ethanol; dichloromethane; dimethyl sulfoxide; 1,2-dichloro-ethane;
DOI:10.1248/cpb.33.4422
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 95 percent / dimethylsulfoxide / 15 h / 80 °C
2: 86 percent / NaOH, 3N HCl / ethanol / 19 h / Heating
3: PCl5 / CH2Cl2 / 2 h / 25 °C
4: 44 percent / AlCl3 / 1,2-dichloro-ethane / 72 h / 20 °C
5: 79 percent / NaOH / methanol / 2 h / Ambient temperature
6: H2, 70percent HClO4 / 5percent Pd-C / 24 h / Ambient temperature
With
hydrogenchloride; sodium hydroxide; aluminium trichloride; perchloric acid; phosphorus pentachloride; hydrogen;
palladium on activated charcoal;
In
methanol; ethanol; dichloromethane; dimethyl sulfoxide; 1,2-dichloro-ethane;
DOI:10.1248/cpb.33.4422
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) NaOH / p-TsOH / 1.) MeOH, reflux, 3 h; 2.) 60 degC, 2 h
2: PCl5 / CH2Cl2 / 2 h / 25 °C
3: 44 percent / AlCl3 / 1,2-dichloro-ethane / 72 h / 20 °C
4: 79 percent / NaOH / methanol / 2 h / Ambient temperature
5: H2, 70percent HClO4 / 5percent Pd-C / 24 h / Ambient temperature
With
sodium hydroxide; aluminium trichloride; perchloric acid; phosphorus pentachloride; hydrogen;
palladium on activated charcoal; toluene-4-sulfonic acid;
In
methanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1248/cpb.33.4422
