2,5-dioxopyrrolidin-1-yl 4-cyano-4-(((ethylthio)carbonothioyl)thio)pentanoate

Base Information

• Chemical Name: 2,5-dioxopyrrolidin-1-yl 4-cyano-4-(((ethylthio)carbonothioyl)thio)pentanoate
• CAS No.: 1195771-65-3
• Molecular Formula: C₁₃H₁₆N₂O₄S₃
• Molecular Weight: 360.479
• Mol file: 1195771-65-3.mol

Synonyms:2,5-dioxopyrrolidin-1-yl 4-cyano-4-(((ethylthio)carbonothioyl)thio)pentanoate

Chemical Property of 2,5-dioxopyrrolidin-1-yl 4-cyano-4-(((ethylthio)carbonothioyl)thio)pentanoate

Chemical Property:

• Boiling Point: 551.1±60.0 °C(Predicted)
• Density: 1.41±0.1 g/cm3(Predicted)
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

99%, ^*data from raw suppliers

2,5-Dioxopyrrolidin-1-yl4-cyano-4-(((ethylthio)carbonothioyl)thio)pentanoate 97% ^*data from reagent suppliers

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Technology Process of 2,5-dioxopyrrolidin-1-yl 4-cyano-4-(((ethylthio)carbonothioyl)thio)pentanoate

There total 1 articles about 2,5-dioxopyrrolidin-1-yl 4-cyano-4-(((ethylthio)carbonothioyl)thio)pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

1-hydroxy-pyrrolidine-2,5-dione (6066-82-6) + cyano-4-[(ethylsulfanylthiocarbonyl)sulfanyl]-4-methylbutanoic acid (1137725-46-2) → 2,5-dioxopyrrolidin-1-yl 4-cyano-4-(((ethylthio)carbonothioyl)thio)pentanoate (1195771-65-3)

Guidance literature:

With dicyclohexyl-carbodiimide; In chloroform; at 0 - 20 ℃; for 23h;

DOI:10.1016/j.tetlet.2018.12.051

Reference yield: 58.0%

2,5-dioxopyrrolidin-1-yl 4-cyano-4-(((ethylthio)carbonothioyl)thio)pentanoate (1195771-65-3) + t-butoxycarbonylaminoethyl-rhodamine B → 7-cyano-7-methyl-4-oxo-9-thioxo-8,10-dithia-3-azadodecanyl-rhodamine B

Guidance literature:

t-butoxycarbonylaminoethyl-rhodamine B; With trifluoroacetic acid; In dichloromethane; at 0 - 5 ℃; for 1h;

2,5-dioxopyrrolidin-1-yl 4-cyano-4-(((ethylthio)carbonothioyl)thio)pentanoate; With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 1h;

upstream raw materials:

1-hydroxy-pyrrolidine-2,5-dione

cyano-4-[(ethylsulfanylthiocarbonyl)sulfanyl]-4-methylbutanoic acid

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