2',3'-dichloro-4-fluoro-4-phenyl-3,4,5,6-tetrahydro-2H-[1,4']bipyridinyl

Base Information

Chemical Name:2',3'-dichloro-4-fluoro-4-phenyl-3,4,5,6-tetrahydro-2H-[1,4']bipyridinyl
CAS No.:1152617-71-4
Molecular Formula:C₁₆H₁₅Cl₂FN₂
Molecular Weight:325.213
Hs Code.:

Synonyms:2',3'-dichloro-4-fluoro-4-phenyl-3,4,5,6-tetrahydro-2H-[1,4']bipyridinyl

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2',3'-dichloro-4-fluoro-4-phenyl-3,4,5,6-tetrahydro-2H-[1,4']bipyridinyl

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Technology Process of 2',3'-dichloro-4-fluoro-4-phenyl-3,4,5,6-tetrahydro-2H-[1,4']bipyridinyl

There total 1 articles about 2',3'-dichloro-4-fluoro-4-phenyl-3,4,5,6-tetrahydro-2H-[1,4']bipyridinyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 889865-45-6
2,3-dichloro-4-iodopyridine

: 1056382-25-2
4-fluoro-4-phenylpiperidine hydrochloride

: 1152617-71-4
2',3'-dichloro-4-fluoro-4-phenyl-3,4,5,6-tetrahydro-2H-[1,4']bipyridinyl

Guidance literature:: 2,3-dichloro-4-iodopyridine; 4-fluoro-4-phenylpiperidine hydrochloride; In N,N-dimethyl-formamide; acetonitrile; at 110 ℃; for 6h; sealed tube;

With sodium hydrogencarbonate; In water; N,N-dimethyl-formamide; acetonitrile;

Reference yield: 84.0%

: 1152617-71-4
2',3'-dichloro-4-fluoro-4-phenyl-3,4,5,6-tetrahydro-2H-[1,4']bipyridinyl

: 1254981-22-0
(3'-chloro-4-fluoro-4-phenyl-3,4,5,6-tetrahydro-2H-[1,4']bipyridinyl-2'-yl)hydrazine

Guidance literature:: With hydrazine hydrate; In ethanol; at 160 ℃; for 0.333333h; Microwave irradiation;

Reference yield:

: 1152617-71-4
2',3'-dichloro-4-fluoro-4-phenyl-3,4,5,6-tetrahydro-2H-[1,4']bipyridinyl

: 1152617-73-6
2-amino-3-chloro-4-(4'-fluoro-4'-phenyl)piperidinylpyridine

Guidance literature:: 2',3'-dichloro-4-fluoro-4-phenyl-3,4,5,6-tetrahydro-2H-[1,4']bipyridinyl; With Benzophenone imine; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In toluene; at 80 ℃; for 16h; sealed tube;

With hydroxylamine hydrochloride; triethylamine; In methanol; toluene; for 5h;