13-cyclohexyl-3-methoxy-6-(2-{methyl-[2-(2-nitro-benzenesulfonylamino)-ethyl]-amino}-ethylcarbamoyl)-7H-benzo[3,4]azepino[1,2-a]indole-10-carboxylic acid tert-butyl ester

Base Information

• Chemical Name: 13-cyclohexyl-3-methoxy-6-(2-{methyl-[2-(2-nitro-benzenesulfonylamino)-ethyl]-amino}-ethylcarbamoyl)-7H-benzo[3,4]azepino[1,2-a]indole-10-carboxylic acid tert-butyl ester
• CAS No.: 1204417-34-4
• Molecular Formula: C₄₁H₄₉N₅O₈S
• Molecular Weight: 771.935

Synonyms:13-cyclohexyl-3-methoxy-6-(2-{methyl-[2-(2-nitro-benzenesulfonylamino)-ethyl]-amino}-ethylcarbamoyl)-7H-benzo[3,4]azepino[1,2-a]indole-10-carboxylic acid tert-butyl ester

Chemical Property of 13-cyclohexyl-3-methoxy-6-(2-{methyl-[2-(2-nitro-benzenesulfonylamino)-ethyl]-amino}-ethylcarbamoyl)-7H-benzo[3,4]azepino[1,2-a]indole-10-carboxylic acid tert-butyl ester

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Technology Process of 13-cyclohexyl-3-methoxy-6-(2-{methyl-[2-(2-nitro-benzenesulfonylamino)-ethyl]-amino}-ethylcarbamoyl)-7H-benzo[3,4]azepino[1,2-a]indole-10-carboxylic acid tert-butyl ester

There total 1 articles about 13-cyclohexyl-3-methoxy-6-(2-{methyl-[2-(2-nitro-benzenesulfonylamino)-ethyl]-amino}-ethylcarbamoyl)-7H-benzo[3,4]azepino[1,2-a]indole-10-carboxylic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

7H-indolo[2,1-a][2]benzazepine-6,10-dicarboxylic acid, 13-cyclohexyl-3-methoxy-, 10-(1,1-dimethylethyl) ester (1038924-00-3) + N-(2-((2-aminoethyl)(methyl)-amino)ethyl)-2-nitrobenzenesulfonamide (1204417-32-2) → 13-cyclohexyl-3-methoxy-6-(2-{methyl-[2-(2-nitro-benzenesulfonylamino)-ethyl]-amino}-ethylcarbamoyl)-7H-benzo[3,4]azepino[1,2-a]indole-10-carboxylic acid tert-butyl ester (1204417-34-4)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

Reference yield: 83.0%

13-cyclohexyl-3-methoxy-6-(2-{methyl-[2-(2-nitro-benzenesulfonylamino)-ethyl]-amino}-ethylcarbamoyl)-7H-benzo[3,4]azepino[1,2-a]indole-10-carboxylic acid tert-butyl ester (1204417-34-4) + methyl iodide (74-88-4) → 13-cyclohexyl-3-methoxy-6-[2-(methyl-{2-[methyl-(2-nitro-benzenesulfonyl)-amino]-ethyl}-amino)-ethylcarbamoyl]-7H-benzo[3,4]azepino[1,2-a]indole-10-carboxylic acid tert-butyl ester (1204417-35-5)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

upstream raw materials:

7H-indolo[2,1-a][2]benzazepine-6,10-dicarboxylic acid, 13-cyclohexyl-3-methoxy-, 10-(1,1-dimethylethyl) ester

N-(2-((2-aminoethyl)(methyl)-amino)ethyl)-2-nitrobenzenesulfonamide

Downstream raw materials:

13-cyclohexyl-3-methoxy-6-[2-(methyl-{2-[methyl-(2-nitro-benzenesulfonyl)-amino]-ethyl}-amino)-ethylcarbamoyl]-7H-benzo[3,4]azepino[1,2-a]indole-10-carboxylic acid tert-butyl ester

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