(MeCp)2MoO

Base Information

• Chemical Name: (MeCp)2MoO
• CAS No.: 98525-67-8
• Molecular Formula: C₁₂H₁₄MoO
• Molecular Weight: 270.183
• Mol file: 98525-67-8.mol

Synonyms:(MeCp)2MoO

Chemical Property of (MeCp)2MoO

Chemical Property:

Purity/Quality:

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Technology Process of (MeCp)2MoO

There total 1 articles about (MeCp)2MoO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

[((Me)Cp)2MoH2] (61112-91-2) + water (7732-18-5) → (MeCp)2MoO (98525-67-8) + hydrogen (1333-74-0)

Guidance literature:

In water; acetonitrile; Irradiation (UV/VIS); under N2 or Ar, std. Schlenk or vac. techniques; irradiated (λ>350 nm) for 24 h; solvent removed in vac.; UV/Vis; NMR; gas manometric measurements;

DOI:10.1016/S0020-1693(99)00541-1

Reference yield: 79.0%

(MeCp)2MoO (98525-67-8) + tris(pentafluorophenyl)borate (1109-15-5) → [Mo(C5H4CH3)2OB(C6F5)3]

Guidance literature:

In toluene; (N2); stirring (2 h); removal of solvent (vac.), washing (pentane), extn. (toluene), concn., crystn. on cooling to -20°C; elem. anal.;

upstream raw materials:

[((Me)Cp)2MoH₂]

water