(S)-3-(2-bromo-5-(tert-butyldimethylsilyloxy)-4-methoxy-3-methylphenyl)-2-(tert-butoxycarbonylamino)propanoic acid

Base Information

Chemical Name:(S)-3-(2-bromo-5-(tert-butyldimethylsilyloxy)-4-methoxy-3-methylphenyl)-2-(tert-butoxycarbonylamino)propanoic acid
CAS No.:1177255-37-6
Molecular Formula:C₂₂H₃₆BrNO₆Si
Molecular Weight:518.52
Hs Code.:

Synonyms:(S)-3-(2-bromo-5-(tert-butyldimethylsilyloxy)-4-methoxy-3-methylphenyl)-2-(tert-butoxycarbonylamino)propanoic acid

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Chemical Property of (S)-3-(2-bromo-5-(tert-butyldimethylsilyloxy)-4-methoxy-3-methylphenyl)-2-(tert-butoxycarbonylamino)propanoic acid

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Technology Process of (S)-3-(2-bromo-5-(tert-butyldimethylsilyloxy)-4-methoxy-3-methylphenyl)-2-(tert-butoxycarbonylamino)propanoic acid

There total 1 articles about (S)-3-(2-bromo-5-(tert-butyldimethylsilyloxy)-4-methoxy-3-methylphenyl)-2-(tert-butoxycarbonylamino)propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1177255-36-5
C₁₆H₂₂BrNO₆

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1177255-37-6
(S)-3-(2-bromo-5-(tert-butyldimethylsilyloxy)-4-methoxy-3-methylphenyl)-2-(tert-butoxycarbonylamino)propanoic acid

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 48h;
DOI:10.1016/j.tet.2009.05.025

Reference yield: 88.0%

: 1177255-37-6
(S)-3-(2-bromo-5-(tert-butyldimethylsilyloxy)-4-methoxy-3-methylphenyl)-2-(tert-butoxycarbonylamino)propanoic acid

: 1177255-33-2
(1R,3S)-1-(benzyloxymethyl)-5-bromo-8-(tert-butyldimethylsilyloxy)-3-((tert-butyldimethylsilyloxy)methyl)-7-methoxy-6-methyl-1,2,3,4-tetrahydroisoquinoline

: 1177255-38-7
C₅₄H₈₆Br₂N₂O₉Si₃

Guidance literature:: With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1016/j.tet.2009.05.025

Reference yield: 88.0%

: 1177255-37-6
(S)-3-(2-bromo-5-(tert-butyldimethylsilyloxy)-4-methoxy-3-methylphenyl)-2-(tert-butoxycarbonylamino)propanoic acid

: 1310875-40-1
benzyl ((1R,3S)-8-(tert-butyldimethylsilyloxy)-3-((tert-butyldimethylsilyloxy)methyl)-7-methoxy-6-methyl-1,2,3,4-tetrahydroisoquinolin-1-yl)methylcarbamate

: 1310875-41-2
C₅₅H₈₈BrN₃O₁₀Si₃

Guidance literature:: With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine; In dichloromethane; at 20 ℃; for 72h; Cooling with ice;
DOI:10.1021/jo200758r