(1R,3S)-1-(benzyloxymethyl)-5-bromo-8-(tert-butyldimethylsilyloxy)-3-((tert-butyldimethylsilyloxy)methyl)-7-methoxy-6-methyl-1,2,3,4-tetrahydroisoquinoline

Base Information

Chemical Name:(1R,3S)-1-(benzyloxymethyl)-5-bromo-8-(tert-butyldimethylsilyloxy)-3-((tert-butyldimethylsilyloxy)methyl)-7-methoxy-6-methyl-1,2,3,4-tetrahydroisoquinoline
CAS No.:1177255-33-2
Molecular Formula:C₃₂H₅₂BrNO₄Si₂
Molecular Weight:650.844
Hs Code.:

(1R,3S)-1-(benzyloxymethyl)-5-bromo-8-(tert-butyldimethylsilyloxy)-3-((tert-butyldimethylsilyloxy)methyl)-7-methoxy-6-methyl-1,2,3,4-tetrahydroisoquinoline

Synonyms:(1R,3S)-1-(benzyloxymethyl)-5-bromo-8-(tert-butyldimethylsilyloxy)-3-((tert-butyldimethylsilyloxy)methyl)-7-methoxy-6-methyl-1,2,3,4-tetrahydroisoquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,3S)-1-(benzyloxymethyl)-5-bromo-8-(tert-butyldimethylsilyloxy)-3-((tert-butyldimethylsilyloxy)methyl)-7-methoxy-6-methyl-1,2,3,4-tetrahydroisoquinoline

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Technology Process of (1R,3S)-1-(benzyloxymethyl)-5-bromo-8-(tert-butyldimethylsilyloxy)-3-((tert-butyldimethylsilyloxy)methyl)-7-methoxy-6-methyl-1,2,3,4-tetrahydroisoquinoline

There total 1 articles about (1R,3S)-1-(benzyloxymethyl)-5-bromo-8-(tert-butyldimethylsilyloxy)-3-((tert-butyldimethylsilyloxy)methyl)-7-methoxy-6-methyl-1,2,3,4-tetrahydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1177255-32-1
(1R,3S)-1-(benzyloxymethyl)-5-bromo-3-(hydroxymethyl)-7-methoxy-6-methyl-1,2,3,4-tetrahydroisoquinolin-8-ol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1177255-33-2
(1R,3S)-1-(benzyloxymethyl)-5-bromo-8-(tert-butyldimethylsilyloxy)-3-((tert-butyldimethylsilyloxy)methyl)-7-methoxy-6-methyl-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: With dmap; triethylamine; In dichloromethane; for 24h;
DOI:10.1016/j.tet.2009.05.025

Reference yield: 88.0%

: 1177255-37-6
(S)-3-(2-bromo-5-(tert-butyldimethylsilyloxy)-4-methoxy-3-methylphenyl)-2-(tert-butoxycarbonylamino)propanoic acid

: 1177255-33-2
(1R,3S)-1-(benzyloxymethyl)-5-bromo-8-(tert-butyldimethylsilyloxy)-3-((tert-butyldimethylsilyloxy)methyl)-7-methoxy-6-methyl-1,2,3,4-tetrahydroisoquinoline

: 1177255-38-7
C₅₄H₈₆Br₂N₂O₉Si₃

Guidance literature:: With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1016/j.tet.2009.05.025