trans-tert-buthyl-2-phenylcyclopropyl carbamate

Base Information

Chemical Name:trans-tert-buthyl-2-phenylcyclopropyl carbamate
CAS No.:185256-49-9
Molecular Formula:C₁₄H₁₉NO₂
Molecular Weight:233.31
Hs Code.:

Synonyms:trans-tert-buthyl-2-phenylcyclopropyl carbamate

Suppliers and Price of trans-tert-buthyl-2-phenylcyclopropyl carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of trans-tert-buthyl-2-phenylcyclopropyl carbamate

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of trans-tert-buthyl-2-phenylcyclopropyl carbamate

There total 5 articles about trans-tert-buthyl-2-phenylcyclopropyl carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.0%

: 23020-15-7
(1S,2S)-2-phenylcyclopropane-1-carboxylic acid

: 75-65-0
tert-butyl alcohol

: 185256-49-9,847644-86-4
trans-tert-buthyl-2-phenylcyclopropyl carbamate

: (+)-(1S,2R)-trans (2-phenyl-cyclopropyl)-carbamoyl azide

Guidance literature:: With diphenyl phosphoryl azide; triethylamine; at 90 - 95 ℃; for 5h;
DOI:10.1016/S0957-4166(96)00457-0

Reference yield:

: 847644-86-4
((1SR,2RS)-tert-butyl-2-phenylcyclopropyl)carbamate

: 185256-47-7,847644-86-4
(-)-(1R,2S)-trans (2-phenyl-cyclopropyl)carbaminic acid tert-butyl ester

: 185256-49-9,847644-86-4
trans-tert-buthyl-2-phenylcyclopropyl carbamate

Guidance literature:: With Chiralcel OJ polysaccharide-based chiral stationary phase; In ethanol; hexane; at 25 ℃; optical yield given as %ee; Resolution of racemate;
DOI:10.1021/ja101557k