C₁₄H₁₉NO₆

Base Information

Chemical Name:C₁₄H₁₉NO₆
CAS No.:1354688-32-6
Molecular Formula:C₁₄H₁₉NO₆
Molecular Weight:297.308
Hs Code.:

C<sub>14</sub>H<sub>19</sub>NO<sub>6</sub>

Synonyms:C₁₄H₁₉NO₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₉NO₆

Chemical Property:

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Technology Process of C₁₄H₁₉NO₆

There total 3 articles about C₁₄H₁₉NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1354688-31-5
C₁₄H₂₀O₄

: 1354688-32-6
C₁₄H₁₉NO₆

Guidance literature:: With clay-supported copper(II) nitrate; In tetrachloromethane; acetic anhydride; at 0 ℃; for 1.5h; regioselective reaction;
DOI:10.1055/s-0031-1289551

Reference yield:

: 74866-17-4
3,4-dimethoxy-2-methyl-1-bromobenzene

: 1354688-32-6
C₁₄H₁₉NO₆

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C

1.2: 18 h / -78 °C

2.1: dmap; triethylamine / dichloromethane / 2 h / 20 °C

3.1: clay-supported copper(II) nitrate / tetrachloromethane; acetic anhydride / 1.5 h / 0 °C

With dmap; n-butyllithium; triethylamine; In tetrahydrofuran; tetrachloromethane; dichloromethane; acetic anhydride;
DOI:10.1055/s-0031-1289551

Reference yield:

: 4463-33-6
1,2-dimethoxy-3-methylbenzene

: 1354688-32-6
C₁₄H₁₉NO₆

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-Bromosuccinimide / acetonitrile / 27 h / 20 °C

2.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C

2.2: 18 h / -78 °C

3.1: dmap; triethylamine / dichloromethane / 2 h / 20 °C

4.1: clay-supported copper(II) nitrate / tetrachloromethane; acetic anhydride / 1.5 h / 0 °C

With dmap; N-Bromosuccinimide; n-butyllithium; triethylamine; In tetrahydrofuran; tetrachloromethane; dichloromethane; acetic anhydride; acetonitrile;
DOI:10.1055/s-0031-1289551