1-benzyloxy-3-carboxy-2-carboxymethylnaphthalene diethylester

Base Information

• Chemical Name: 1-benzyloxy-3-carboxy-2-carboxymethylnaphthalene diethylester
• CAS No.: 852238-09-6
• Molecular Formula: C₂₄H₂₄O₅
• Molecular Weight: 392.452
• Mol file: 852238-09-6.mol

Synonyms:1-benzyloxy-3-carboxy-2-carboxymethylnaphthalene diethylester

Chemical Property of 1-benzyloxy-3-carboxy-2-carboxymethylnaphthalene diethylester

Chemical Property:

Purity/Quality:

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Technology Process of 1-benzyloxy-3-carboxy-2-carboxymethylnaphthalene diethylester

There total 1 articles about 1-benzyloxy-3-carboxy-2-carboxymethylnaphthalene diethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

3-carboxy-2-carboxymethyl-1-naphthol diethylester (852238-08-5) + benzyl bromide (100-39-0) → 1-benzyloxy-3-carboxy-2-carboxymethylnaphthalene diethylester (852238-09-6)

Guidance literature:

With potassium carbonate; In acetone; for 24h; Heating;

DOI:10.1002/jhet.5570420220

Reference yield: 95.0%

1-benzyloxy-3-carboxy-2-carboxymethylnaphthalene diethylester (852238-09-6) → 1-benzyloxy-3-carboxy-2-carboxymethylnaphthalene (852238-10-9)

Guidance literature:

With potassium hydroxide; In methanol; for 6h; Heating;

DOI:10.1002/jhet.5570420220

Reference yield:

1-benzyloxy-3-carboxy-2-carboxymethylnaphthalene diethylester (852238-09-6) → 9-benzyloxybenzo[f]isochroman-1,3-dione (852238-11-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / KOH / methanol / 6 h / Heating

2: 89 percent / acetyl chloride / 12 h / Heating

With potassium hydroxide; acetyl chloride; In methanol;

DOI:10.1002/jhet.5570420220

upstream raw materials:

3-carboxy-2-carboxymethyl-1-naphthol diethylester

benzyl bromide

Downstream raw materials:

1-benzyloxy-3-carboxy-2-carboxymethylnaphthalene

9-benzyloxybenzo[f]isochroman-1,3-dione