potassium 2-(((1r,4r)-4-(((3-fluorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetate

Base Information

Chemical Name:potassium 2-(((1r,4r)-4-(((3-fluorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetate
CAS No.:1187857-78-8
Molecular Formula:C₂₃H₂₅FNO₅*K
Molecular Weight:453.552
Hs Code.:

Synonyms:potassium 2-(((1r,4r)-4-(((3-fluorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetate

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Chemical Property of potassium 2-(((1r,4r)-4-(((3-fluorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetate

Chemical Property:

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Technology Process of potassium 2-(((1r,4r)-4-(((3-fluorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetate

There total 11 articles about potassium 2-(((1r,4r)-4-(((3-fluorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1187856-50-3
2-(((1r,4r)-4-(((3-fluorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetic acid

: 584-08-7
potassium carbonate

: 1187857-78-8
potassium 2-(((1r,4r)-4-(((3-fluorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetate

Guidance literature:: In water; isopropyl alcohol; at 20 ℃; for 0.25h;

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 1187857-78-8
potassium 2-(((1r,4r)-4-(((3-fluorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetate

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium t-butanolate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / toluene / 3 h / 105 °C

2.1: pyridine / 0 - 25 °C / Inert atmosphere

3.1: acetonitrile / 20 °C / Heating

4.1: dmap / acetonitrile / 18 h / 53 °C

5.1: rhodium(II) acetate / dichloromethane / 4 - 30 °C

6.1: lithium bromide / acetonitrile

6.2: 2 h / 70 °C

7.1: water; isopropyl alcohol / 0.25 h / 20 °C

With pyridine; dmap; lithium bromide; sodium t-butanolate; rhodium(II) acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In dichloromethane; water; isopropyl alcohol; toluene; acetonitrile;

Reference yield:

: 372-19-0
meta-fluoroaniline

: 1187857-78-8
potassium 2-(((1r,4r)-4-(((3-fluorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetate

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium t-butanolate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / toluene / 3 h / 105 °C

2.1: pyridine / 0 - 25 °C / Inert atmosphere

3.1: acetonitrile / 20 °C / Heating

4.1: dmap / acetonitrile / 18 h / 53 °C

5.1: rhodium(II) acetate / dichloromethane / 4 - 30 °C

6.1: lithium bromide / acetonitrile

6.2: 2 h / 70 °C

7.1: water; isopropyl alcohol / 0.25 h / 20 °C

With pyridine; dmap; lithium bromide; sodium t-butanolate; rhodium(II) acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In dichloromethane; water; isopropyl alcohol; toluene; acetonitrile;