(2S,3S,4R)-1-benzyl-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-5-C-methylene piperidine

Base Information

Chemical Name:(2S,3S,4R)-1-benzyl-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-5-C-methylene piperidine
CAS No.:1161011-52-4
Molecular Formula:C₃₅H₃₇NO₃
Molecular Weight:519.684
Hs Code.:

Synonyms:(2S,3S,4R)-1-benzyl-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-5-C-methylene piperidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S,4R)-1-benzyl-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-5-C-methylene piperidine

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Technology Process of (2S,3S,4R)-1-benzyl-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-5-C-methylene piperidine

There total 2 articles about (2S,3S,4R)-1-benzyl-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-5-C-methylene piperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1161011-51-3
(2S,3S,4R)-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-5-methylenepiperidine

: 100-39-0
benzyl bromide

: 1161011-52-4
(2S,3S,4R)-1-benzyl-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-5-C-methylene piperidine

Guidance literature:: With potassium carbonate; In acetonitrile; at 20 ℃; for 4h;
DOI:10.1002/ejoc.200801301

Reference yield:

: 1265884-08-9
(3R,4R,5R)-3,4,6-tris(benzyloxy)-5-(methylsulfonyloxy)-2-(methylsulfonyloxymethyl)-hex-1-ene

: 100-46-9
benzylamine

: 1161011-52-4
(2S,3S,4R)-1-benzyl-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-5-C-methylene piperidine

Guidance literature:: at 90 ℃; for 26h; Neat (no solvent);
DOI:10.1016/j.tet.2010.11.050

Reference yield: 93.0%

: 1161011-52-4
(2S,3S,4R)-1-benzyl-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-5-C-methylene piperidine

: 1161011-53-5
(2S,3S,4S,5R)-1-benzyl-2-(benzyloxymethyl)-3,4-bis(benzyloxy)-5-(hydroxymethyl)piperidin-5-ol

Guidance literature:: With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In water; acetone; tert-butyl alcohol; at 20 ℃; for 48h;
DOI:10.1002/ejoc.200801301