(2S,3S,4R)-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-5-methylenepiperidine

Base Information

Chemical Name:(2S,3S,4R)-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-5-methylenepiperidine
CAS No.:1161011-51-3
Molecular Formula:C₂₈H₃₁NO₃
Molecular Weight:429.559
Hs Code.:

Synonyms:(2S,3S,4R)-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-5-methylenepiperidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S,4R)-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-5-methylenepiperidine

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Technology Process of (2S,3S,4R)-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-5-methylenepiperidine

There total 1 articles about (2S,3S,4R)-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-5-methylenepiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.5%

: 1161011-50-2
tert-butyl (3R,4R,5R)-3,4,6-tris(benzyloxy)-5-(methylsulfonyloxy)-2-methylenehexylcarbamate

: 1161011-51-3
(2S,3S,4R)-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-5-methylenepiperidine

Guidance literature:: tert-butyl (3R,4R,5R)-3,4,6-tris(benzyloxy)-5-(methylsulfonyloxy)-2-methylenehexylcarbamate; With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 0.833333h;

With potassium carbonate; In acetonitrile; at 20 - 70 ℃; for 8h;
DOI:10.1002/ejoc.200801301