4-((1-methyl-1H-benzo[d][1,2,3]triazol-6-yl)(1H-1,2,4-triazol-1-yl)methyl)phenol

Base Information

Chemical Name:4-((1-methyl-1H-benzo[d][1,2,3]triazol-6-yl)(1H-1,2,4-triazol-1-yl)methyl)phenol
CAS No.:1331740-83-0
Molecular Formula:C₁₆H₁₄N₆O
Molecular Weight:306.327
Hs Code.:

Synonyms:4-((1-methyl-1H-benzo[d][1,2,3]triazol-6-yl)(1H-1,2,4-triazol-1-yl)methyl)phenol

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Chemical Property of 4-((1-methyl-1H-benzo[d][1,2,3]triazol-6-yl)(1H-1,2,4-triazol-1-yl)methyl)phenol

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Technology Process of 4-((1-methyl-1H-benzo[d][1,2,3]triazol-6-yl)(1H-1,2,4-triazol-1-yl)methyl)phenol

There total 8 articles about 4-((1-methyl-1H-benzo[d][1,2,3]triazol-6-yl)(1H-1,2,4-triazol-1-yl)methyl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1331740-82-9
6-((4-benzyloxyphenyl)(1H-1,2,4-triazol-1-yl)methyl)-1-methyl-1H-benzo[d][1,2,3]triazole

: 1331740-83-0
4-((1-methyl-1H-benzo[d][1,2,3]triazol-6-yl)(1H-1,2,4-triazol-1-yl)methyl)phenol

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; methanol; at 20 ℃;
DOI:10.1002/cmdc.201100145

Reference yield:

: 66630-74-8
4-amino-3-(methylamino)benzoic acid

: 1331740-83-0
4-((1-methyl-1H-benzo[d][1,2,3]triazol-6-yl)(1H-1,2,4-triazol-1-yl)methyl)phenol

Guidance literature:: Multi-step reaction with 8 steps

1.1: hydrogenchloride; sodium nitrite / water / 0 - 20 °C

2.1: thionyl chloride / Reflux

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.33 h / 20 °C

4.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trichloroisocyanuric acid / dichloromethane / 0.17 h / 0 °C

5.1: iodine; magnesium / tetrahydrofuran / Heating

5.2: 20 °C

6.1: thionyl chloride / dichloromethane / 2 h / 20 °C

7.1: potassium carbonate; potassium iodide / acetone / 60 °C

8.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; methanol / 20 °C

With hydrogenchloride; lithium aluminium tetrahydride; thionyl chloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trichloroisocyanuric acid; palladium 10% on activated carbon; hydrogen; iodine; potassium carbonate; magnesium; potassium iodide; sodium nitrite; In tetrahydrofuran; methanol; dichloromethane; water; acetone;
DOI:10.1002/cmdc.201100145

Reference yield:

: 1-methyl-1H-benzo[d][1,2,3]triazole-6-carboxylic acid

: 1331740-83-0
4-((1-methyl-1H-benzo[d][1,2,3]triazol-6-yl)(1H-1,2,4-triazol-1-yl)methyl)phenol

Guidance literature:: Multi-step reaction with 7 steps

1.1: thionyl chloride / Reflux

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.33 h / 20 °C

3.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trichloroisocyanuric acid / dichloromethane / 0.17 h / 0 °C

4.1: iodine; magnesium / tetrahydrofuran / Heating

4.2: 20 °C

5.1: thionyl chloride / dichloromethane / 2 h / 20 °C

6.1: potassium carbonate; potassium iodide / acetone / 60 °C

7.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; methanol / 20 °C

With lithium aluminium tetrahydride; thionyl chloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trichloroisocyanuric acid; palladium 10% on activated carbon; hydrogen; iodine; potassium carbonate; magnesium; potassium iodide; In tetrahydrofuran; methanol; dichloromethane; acetone;
DOI:10.1002/cmdc.201100145