4-((1-methyl-1H-benzo[d][1,2,3]triazol-6-yl)(1H-1,2,4-triazol-1-yl)methyl)phenyl sulfamate

Base Information

Chemical Name:4-((1-methyl-1H-benzo[d][1,2,3]triazol-6-yl)(1H-1,2,4-triazol-1-yl)methyl)phenyl sulfamate
CAS No.:1331740-84-1
Molecular Formula:C₁₆H₁₅N₇O₃S
Molecular Weight:385.406
Hs Code.:

Synonyms:4-((1-methyl-1H-benzo[d][1,2,3]triazol-6-yl)(1H-1,2,4-triazol-1-yl)methyl)phenyl sulfamate

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Chemical Property of 4-((1-methyl-1H-benzo[d][1,2,3]triazol-6-yl)(1H-1,2,4-triazol-1-yl)methyl)phenyl sulfamate

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Technology Process of 4-((1-methyl-1H-benzo[d][1,2,3]triazol-6-yl)(1H-1,2,4-triazol-1-yl)methyl)phenyl sulfamate

There total 8 articles about 4-((1-methyl-1H-benzo[d][1,2,3]triazol-6-yl)(1H-1,2,4-triazol-1-yl)methyl)phenyl sulfamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1331740-83-0
4-((1-methyl-1H-benzo[d][1,2,3]triazol-6-yl)(1H-1,2,4-triazol-1-yl)methyl)phenol

: 1331740-84-1
4-((1-methyl-1H-benzo[d][1,2,3]triazol-6-yl)(1H-1,2,4-triazol-1-yl)methyl)phenyl sulfamate

Guidance literature:: With sulphamoyl chloride; In N,N-dimethyl acetamide; at 20 ℃; Cooling with ice;
DOI:10.1002/cmdc.201100145

Reference yield:

: 66630-74-8
4-amino-3-(methylamino)benzoic acid

: 1331740-84-1
4-((1-methyl-1H-benzo[d][1,2,3]triazol-6-yl)(1H-1,2,4-triazol-1-yl)methyl)phenyl sulfamate

Guidance literature:: Multi-step reaction with 9 steps

1.1: hydrogenchloride; sodium nitrite / water / 0 - 20 °C

2.1: thionyl chloride / Reflux

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.33 h / 20 °C

4.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trichloroisocyanuric acid / dichloromethane / 0.17 h / 0 °C

5.1: iodine; magnesium / tetrahydrofuran / Heating

5.2: 20 °C

6.1: thionyl chloride / dichloromethane / 2 h / 20 °C

7.1: potassium carbonate; potassium iodide / acetone / 60 °C

8.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; methanol / 20 °C

9.1: sulphamoyl chloride / N,N-dimethyl acetamide / 20 °C / Cooling with ice

With hydrogenchloride; lithium aluminium tetrahydride; thionyl chloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trichloroisocyanuric acid; palladium 10% on activated carbon; sulphamoyl chloride; hydrogen; iodine; potassium carbonate; magnesium; potassium iodide; sodium nitrite; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl acetamide; water; acetone;
DOI:10.1002/cmdc.201100145

Reference yield:

: 147137-38-0
1-Methyl-1H-benzotriazole-6-carboxylic acid methyl ester

: 1331740-84-1
4-((1-methyl-1H-benzo[d][1,2,3]triazol-6-yl)(1H-1,2,4-triazol-1-yl)methyl)phenyl sulfamate

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.33 h / 20 °C

2.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trichloroisocyanuric acid / dichloromethane / 0.17 h / 0 °C

3.1: iodine; magnesium / tetrahydrofuran / Heating

3.2: 20 °C

4.1: thionyl chloride / dichloromethane / 2 h / 20 °C

5.1: potassium carbonate; potassium iodide / acetone / 60 °C

6.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; methanol / 20 °C

7.1: sulphamoyl chloride / N,N-dimethyl acetamide / 20 °C / Cooling with ice

With lithium aluminium tetrahydride; thionyl chloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trichloroisocyanuric acid; palladium 10% on activated carbon; sulphamoyl chloride; hydrogen; iodine; potassium carbonate; magnesium; potassium iodide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl acetamide; acetone;
DOI:10.1002/cmdc.201100145