14,15,17,18-Tetramethyl-N,N',N'',N'''-tetratosyl-2,5,8,11-tetraaza<12>paracyclophane

Base Information

Chemical Name:14,15,17,18-Tetramethyl-N,N',N'',N'''-tetratosyl-2,5,8,11-tetraaza<12>paracyclophane
CAS No.:150059-49-7
Molecular Formula:C₄₆H₅₆N₄O₈S₄
Molecular Weight:921.237
Hs Code.:

Synonyms:14,15,17,18-Tetramethyl-N,N',N'',N'''-tetratosyl-2,5,8,11-tetraaza<12>paracyclophane

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Chemical Property of 14,15,17,18-Tetramethyl-N,N',N'',N'''-tetratosyl-2,5,8,11-tetraaza<12>paracyclophane

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Technology Process of 14,15,17,18-Tetramethyl-N,N',N'',N'''-tetratosyl-2,5,8,11-tetraaza<12>paracyclophane

There total 3 articles about 14,15,17,18-Tetramethyl-N,N',N'',N'''-tetratosyl-2,5,8,11-tetraaza<12>paracyclophane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 35168-64-0
1,4-bis(bromomethyl)-2,3,5,6-tetramethylbenzene

: 55442-07-4
N,N',N'',N'''-tetrakis-(p-tolylsulphonyl)-triethylenetetramine

: 150059-49-7
14,15,17,18-Tetramethyl-N,N',N'',N'''-tetratosyl-2,5,8,11-tetraaza<12>paracyclophane

Guidance literature:: With potassium carbonate; In acetonitrile; for 24h; Heating;
DOI:10.1021/jo00069a049

Reference yield:

: 112-24-3
triethylentetramine

: 150059-49-7
14,15,17,18-Tetramethyl-N,N',N'',N'''-tetratosyl-2,5,8,11-tetraaza<12>paracyclophane

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / aq. NaOH / tetrahydrofuran / 4 h / 60 °C

2: 71 percent / K₂CO₃ / acetonitrile / 24 h / Heating

With sodium hydroxide; potassium carbonate; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jo00069a049

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 150059-49-7
14,15,17,18-Tetramethyl-N,N',N'',N'''-tetratosyl-2,5,8,11-tetraaza<12>paracyclophane

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / aq. NaOH / tetrahydrofuran / 4 h / 60 °C

2: 71 percent / K₂CO₃ / acetonitrile / 24 h / Heating

With sodium hydroxide; potassium carbonate; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jo00069a049