ethyl 2-(2-carbamoyl-4-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)phenoxy)acetate

Base Information

Chemical Name:ethyl 2-(2-carbamoyl-4-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)phenoxy)acetate
CAS No.:1445854-27-2
Molecular Formula:C₂₉H₄₁NO₆
Molecular Weight:499.648
Hs Code.:

Synonyms:ethyl 2-(2-carbamoyl-4-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)phenoxy)acetate

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Chemical Property of ethyl 2-(2-carbamoyl-4-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)phenoxy)acetate

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Technology Process of ethyl 2-(2-carbamoyl-4-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)phenoxy)acetate

There total 10 articles about ethyl 2-(2-carbamoyl-4-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)phenoxy)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1445854-26-1
2-hydroxy-5-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)benzamide

: 105-36-2
ethyl bromoacetate

: 1445854-27-2
ethyl 2-(2-carbamoyl-4-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)phenoxy)acetate

Guidance literature:: With potassium carbonate; In acetonitrile; at 20 ℃; for 12h;
DOI:10.1016/j.bmc.2015.05.011

Reference yield:

: 176240-84-9
methyl 4-(benzyloxy)-3-bromobenzoate

: 1445854-27-2
ethyl 2-(2-carbamoyl-4-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)phenoxy)acetate

Guidance literature:: Multi-step reaction with 9 steps

1.1: Inert atmosphere

2.1: boron trifluoride diethyl etherate / Inert atmosphere

3.1: triethylamine; palladium diacetate; 1,3-bis-(diphenylphosphino)propane / Inert atmosphere

4.1: potassium carbonate / Inert atmosphere

5.1: sodium tetrahydroborate / Inert atmosphere

6.1: lithium hydroxide / Inert atmosphere

7.1: oxalyl dichloride / Inert atmosphere

7.2: Inert atmosphere

8.1: palladium; hydrogen

9.1: potassium carbonate / Inert atmosphere

With sodium tetrahydroborate; oxalyl dichloride; boron trifluoride diethyl etherate; 1,3-bis-(diphenylphosphino)propane; hydrogen; palladium diacetate; potassium carbonate; palladium; triethylamine; lithium hydroxide;

Reference yield:

: 1445854-17-0
4-(3-(4-(benzyloxy)-3-bromophenyl)pentan-3-yl )-2-methylphenol

: 1445854-27-2
ethyl 2-(2-carbamoyl-4-(3-(4-(2-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)phenoxy)acetate

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylamine; palladium diacetate; 1,3-bis-(diphenylphosphino)propane / Inert atmosphere

2.1: potassium carbonate / Inert atmosphere

3.1: sodium tetrahydroborate / Inert atmosphere

4.1: lithium hydroxide / Inert atmosphere

5.1: oxalyl dichloride / Inert atmosphere

5.2: Inert atmosphere

6.1: palladium; hydrogen

7.1: potassium carbonate / Inert atmosphere

With sodium tetrahydroborate; oxalyl dichloride; 1,3-bis-(diphenylphosphino)propane; hydrogen; palladium diacetate; potassium carbonate; palladium; triethylamine; lithium hydroxide;