(S)-2-[1-Methyl-2-phenyl-eth-(Z)-ylideneamino]-pentanedioic acid diethyl ester

Base Information

Chemical Name:(S)-2-[1-Methyl-2-phenyl-eth-(Z)-ylideneamino]-pentanedioic acid diethyl ester
CAS No.:59903-71-8
Molecular Formula:C₁₈H₂₅NO₄
Molecular Weight:319.401
Hs Code.:

Synonyms:(S)-2-[1-Methyl-2-phenyl-eth-(Z)-ylideneamino]-pentanedioic acid diethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-[1-Methyl-2-phenyl-eth-(Z)-ylideneamino]-pentanedioic acid diethyl ester

Chemical Property:

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Technology Process of (S)-2-[1-Methyl-2-phenyl-eth-(Z)-ylideneamino]-pentanedioic acid diethyl ester

There total 1 articles about (S)-2-[1-Methyl-2-phenyl-eth-(Z)-ylideneamino]-pentanedioic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16450-41-2
L-glutamic acid diethyl ester

: 103-79-7,136675-26-8
1-phenyl-acetone

: 59903-71-8
(S)-2-[1-Methyl-2-phenyl-eth-(Z)-ylideneamino]-pentanedioic acid diethyl ester

Guidance literature:: In benzene; for 48h; Heating;
DOI:10.1248/cpb.31.887

Reference yield:

: 59903-71-8
(S)-2-[1-Methyl-2-phenyl-eth-(Z)-ylideneamino]-pentanedioic acid diethyl ester

: 5965-53-7
diethyl 2-ketoglutarate

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / 5percent palladium on charcoal / ethanol / 16 h / Ambient temperature

2: tert-butyl hypochlorite / diethyl ether / 0.5 h / 0 °C

3: sodium ethoxide / ethanol / 1 h / 40 °C

4: 5percent sulfuric acid / H₂O / 2 h / Ambient temperature

With tert-butylhypochlorite; sulfuric acid; hydrogen; sodium ethanolate; palladium on activated charcoal; In diethyl ether; ethanol; water;
DOI:10.1248/cpb.31.887

Reference yield:

: 59903-71-8
(S)-2-[1-Methyl-2-phenyl-eth-(Z)-ylideneamino]-pentanedioic acid diethyl ester

: 51-64-9,17108-96-2,96332-84-2
dexamfetamine

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / 5percent palladium on charcoal / ethanol / 16 h / Ambient temperature

2: tert-butyl hypochlorite / diethyl ether / 0.5 h / 0 °C

3: sodium ethoxide / ethanol / 1 h / 40 °C

4: 5percent sulfuric acid / H₂O / 2 h / Ambient temperature

With tert-butylhypochlorite; sulfuric acid; hydrogen; sodium ethanolate; palladium on activated charcoal; In diethyl ether; ethanol; water;
DOI:10.1248/cpb.31.887