Technology Process of C8H7BrO3S
There total 4 articles about C8H7BrO3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tert.-butylhydroperoxide; n-butyllithium;
In
tetrahydrofuran; decane; hexane;
at -15 ℃;
Inert atmosphere;
DOI:10.1111/j.1747-0285.2012.01437.x
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium hydroxide / ethanol / Reflux
2: dihydrogen peroxide; sodium tungstate / water
3: triethylamine; methanesulfonyl chloride / tetrahydrofuran / 0 °C / Inert atmosphere
4: n-butyllithium; tert.-butylhydroperoxide / hexane; decane; tetrahydrofuran / -15 °C / Inert atmosphere
With
tert.-butylhydroperoxide; sodium tungstate; n-butyllithium; dihydrogen peroxide; methanesulfonyl chloride; triethylamine; potassium hydroxide;
In
tetrahydrofuran; decane; ethanol; hexane; water;
DOI:10.1111/j.1747-0285.2012.01437.x
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dihydrogen peroxide; sodium tungstate / water
2: triethylamine; methanesulfonyl chloride / tetrahydrofuran / 0 °C / Inert atmosphere
3: n-butyllithium; tert.-butylhydroperoxide / hexane; decane; tetrahydrofuran / -15 °C / Inert atmosphere
With
tert.-butylhydroperoxide; sodium tungstate; n-butyllithium; dihydrogen peroxide; methanesulfonyl chloride; triethylamine;
In
tetrahydrofuran; decane; hexane; water;
DOI:10.1111/j.1747-0285.2012.01437.x