C₆H₅chloro(trifluoroethoxy)borane

Base Information

Chemical Name:C₆H₅chloro(trifluoroethoxy)borane
CAS No.:131252-31-8
Molecular Formula:C₈H₇BClF₃O
Molecular Weight:222.402
Hs Code.:

C<sub>6</sub>H<sub>5</sub>chloro(trifluoroethoxy)borane

Synonyms:C₆H₅chloro(trifluoroethoxy)borane

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Chemical Property of C₆H₅chloro(trifluoroethoxy)borane

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Technology Process of C₆H₅chloro(trifluoroethoxy)borane

There total 1 articles about C₆H₅chloro(trifluoroethoxy)borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 131252-30-7
C₆H₅bis(trifluoroethoxy)borane

: 873-51-8
phenylborondichloride

: 131252-31-8
C₆H₅chloro(trifluoroethoxy)borane

Guidance literature:: molar ratio of educts=1:1, 0°C, stirring overnight; distn., elem. anal.;

Reference yield: 89.0%

: 131252-31-8
C₆H₅chloro(trifluoroethoxy)borane

: 2083-91-2
N,N-Dimethyltrimethylsilylamine

: 131252-34-1
C₆H₅B(N(CH₃)2)OCH₂CF₃

Guidance literature:: In dichloromethane; byproducts: (CH3)3SiCl; 0°C, addn. of Me3SiNMe3, then allowing to warm to room temp., stirring overnight; fractional distn., elem. anal.;

Reference yield: 70.0%

: 131252-31-8
C₆H₅chloro(trifluoroethoxy)borane

: 999-97-3
1,1,1,3,3,3-hexamethyl-disilazane

: 131252-35-2
C₆H₅B(N(Si(CH₃)3)2)OCH₂CF₃

Guidance literature:: With n-butyllithium; In diethyl ether; byproducts: LiCl; 0°C, allowing to warm to room temp. after addn. of n-BuLi to (Me3Si)NH, stirring for 30 min, recooling to 0°C, then addn. of PhBCl(OCH2CF3), stirring overnight; filtration of LiCl under nitrogen, evapn. of the solvent under reduced pressure, distn., elem. anal.;