4-acetoxymethyl-1-benzyloxycarbonyl-4-(4,5-bis(4-methoxyphenyl)oxazol-2-yl)piperidine

Base Information

Chemical Name:4-acetoxymethyl-1-benzyloxycarbonyl-4-(4,5-bis(4-methoxyphenyl)oxazol-2-yl)piperidine
CAS No.:951744-85-7
Molecular Formula:C₃₃H₃₄N₂O₇
Molecular Weight:570.642
Hs Code.:

Synonyms:4-acetoxymethyl-1-benzyloxycarbonyl-4-(4,5-bis(4-methoxyphenyl)oxazol-2-yl)piperidine

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Chemical Property of 4-acetoxymethyl-1-benzyloxycarbonyl-4-(4,5-bis(4-methoxyphenyl)oxazol-2-yl)piperidine

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Technology Process of 4-acetoxymethyl-1-benzyloxycarbonyl-4-(4,5-bis(4-methoxyphenyl)oxazol-2-yl)piperidine

There total 8 articles about 4-acetoxymethyl-1-benzyloxycarbonyl-4-(4,5-bis(4-methoxyphenyl)oxazol-2-yl)piperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 951744-84-6
1-benzyloxycarbonyl-4-(4,5-bis(4-methoxyphenyl)oxazol-2-yl)-4-hydroxymethylpiperidine

: 108-24-7
acetic anhydride

: 951744-85-7
4-acetoxymethyl-1-benzyloxycarbonyl-4-(4,5-bis(4-methoxyphenyl)oxazol-2-yl)piperidine

Guidance literature:: With pyridine; dmap; In dichloromethane; at 20 ℃; for 2h;

Reference yield:

: 27895-95-0
2-bromo-1,2-bis(4-methoxyphenyl)ethanone

: 951744-85-7
4-acetoxymethyl-1-benzyloxycarbonyl-4-(4,5-bis(4-methoxyphenyl)oxazol-2-yl)piperidine

Guidance literature:: Multi-step reaction with 4 steps

1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C

2: ammonium acetate; acetic acid / 17 h / 90 °C

3: lithium borohydride / tetrahydrofuran / 17 h / 20 °C

4: pyridine; dmap / dichloromethane / 2 h / 20 °C

With pyridine; dmap; lithium borohydride; ammonium acetate; caesium carbonate; acetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 120-44-5
1,4-di(4-methoxyphenyl)ethanone

: 951744-85-7
4-acetoxymethyl-1-benzyloxycarbonyl-4-(4,5-bis(4-methoxyphenyl)oxazol-2-yl)piperidine

Guidance literature:: Multi-step reaction with 5 steps

1: pyridinium hydrobromide perbromide / dichloromethane / 1 h / 20 °C

2: caesium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C

3: ammonium acetate; acetic acid / 17 h / 90 °C

4: lithium borohydride / tetrahydrofuran / 17 h / 20 °C

5: pyridine; dmap / dichloromethane / 2 h / 20 °C

With pyridine; dmap; lithium borohydride; pyridinium hydrobromide perbromide; ammonium acetate; caesium carbonate; acetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;