1-benzyloxycarbonyl-4-(4,5-bis(4-methoxyphenyl)oxazol-2-yl)-4-hydroxymethylpiperidine

Base Information

Chemical Name:1-benzyloxycarbonyl-4-(4,5-bis(4-methoxyphenyl)oxazol-2-yl)-4-hydroxymethylpiperidine
CAS No.:951744-84-6
Molecular Formula:C₃₁H₃₂N₂O₆
Molecular Weight:528.605
Hs Code.:

Synonyms:1-benzyloxycarbonyl-4-(4,5-bis(4-methoxyphenyl)oxazol-2-yl)-4-hydroxymethylpiperidine

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Chemical Property of 1-benzyloxycarbonyl-4-(4,5-bis(4-methoxyphenyl)oxazol-2-yl)-4-hydroxymethylpiperidine

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Technology Process of 1-benzyloxycarbonyl-4-(4,5-bis(4-methoxyphenyl)oxazol-2-yl)-4-hydroxymethylpiperidine

There total 7 articles about 1-benzyloxycarbonyl-4-(4,5-bis(4-methoxyphenyl)oxazol-2-yl)-4-hydroxymethylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 951744-37-9
methyl 1-benzyloxycarbonyl-4-(4,5-bis(4-methoxyphenyl)oxazol-2-yl)-4-piperidinecarboxylate

: 951744-84-6
1-benzyloxycarbonyl-4-(4,5-bis(4-methoxyphenyl)oxazol-2-yl)-4-hydroxymethylpiperidine

Guidance literature:: With lithium borohydride; In tetrahydrofuran; at 20 ℃; for 17h;

Reference yield:

: 27895-95-0
2-bromo-1,2-bis(4-methoxyphenyl)ethanone

: 951744-84-6
1-benzyloxycarbonyl-4-(4,5-bis(4-methoxyphenyl)oxazol-2-yl)-4-hydroxymethylpiperidine

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C

2: ammonium acetate; acetic acid / 17 h / 90 °C

3: lithium borohydride / tetrahydrofuran / 17 h / 20 °C

With lithium borohydride; ammonium acetate; caesium carbonate; acetic acid; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 120-44-5
1,4-di(4-methoxyphenyl)ethanone

: 951744-84-6
1-benzyloxycarbonyl-4-(4,5-bis(4-methoxyphenyl)oxazol-2-yl)-4-hydroxymethylpiperidine

Guidance literature:: Multi-step reaction with 4 steps

1: pyridinium hydrobromide perbromide / dichloromethane / 1 h / 20 °C

2: caesium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C

3: ammonium acetate; acetic acid / 17 h / 90 °C

4: lithium borohydride / tetrahydrofuran / 17 h / 20 °C

With lithium borohydride; pyridinium hydrobromide perbromide; ammonium acetate; caesium carbonate; acetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;