2-amino-1,3,5-benzenetricarboxylic acid

Base Information

• Chemical Name: 2-amino-1,3,5-benzenetricarboxylic acid
• CAS No.: 489-96-3
• Molecular Formula: C₉H₇NO₆
• Molecular Weight: 225.158
• Mol file: 489-96-3.mol

Synonyms:2-amino-1,3,5-benzenetricarboxylic acid

Chemical Property of 2-amino-1,3,5-benzenetricarboxylic acid

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-amino-1,3,5-benzenetricarboxylic acid

There total 10 articles about 2-amino-1,3,5-benzenetricarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2-amino-1,3,5-benzenetricarboxylic acid trimethyl ester (15366-35-5) → 2-amino-1,3,5-benzenetricarboxylic acid (489-96-3)

Guidance literature:

With water; potassium hydroxide; In tetrahydrofuran; at 120 ℃; for 0.75h; Microwave irradiation;

DOI:10.1039/c2cc36220a

Reference yield: 83.0%

2-nitro-1,3,5-benzenetricarboxylic acid (19625-68-4) → 2-amino-1,3,5-benzenetricarboxylic acid (489-96-3)

Guidance literature:

With hydrogenchloride; tin; In ethanol; at 50 - 70 ℃; for 2h;

Reference yield:

N-mesitylacetamide (5096-21-9) → 2-amino-1,3,5-benzenetricarboxylic acid (489-96-3)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous KMnO₄; aqueous MgSO₄

2: aqueous H₂SO₄

With potassium permanganate; sulfuric acid; magnesium sulfate;

upstream raw materials:

acetylamino-benzene-1,3,5-tricarboxylic acid

2-nitro-1,3,5-benzenetricarboxylic acid

nitromesitylene

N-mesitylacetamide