5-(2,4,6-Triisopropyl-phenyl)-5-[2,4,6-tris-(bis-trimethylsilanyl-methyl)-phenyl]-[1,2,3,4,5]tetrathiasilolane

Base Information

Chemical Name:5-(2,4,6-Triisopropyl-phenyl)-5-[2,4,6-tris-(bis-trimethylsilanyl-methyl)-phenyl]-[1,2,3,4,5]tetrathiasilolane
CAS No.:160359-06-8
Molecular Formula:C₄₂H₈₂S₄Si₇
Molecular Weight:911.976
Hs Code.:

Synonyms:5-(2,4,6-Triisopropyl-phenyl)-5-[2,4,6-tris-(bis-trimethylsilanyl-methyl)-phenyl]-[1,2,3,4,5]tetrathiasilolane

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Chemical Property of 5-(2,4,6-Triisopropyl-phenyl)-5-[2,4,6-tris-(bis-trimethylsilanyl-methyl)-phenyl]-[1,2,3,4,5]tetrathiasilolane

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Technology Process of 5-(2,4,6-Triisopropyl-phenyl)-5-[2,4,6-tris-(bis-trimethylsilanyl-methyl)-phenyl]-[1,2,3,4,5]tetrathiasilolane

There total 4 articles about 5-(2,4,6-Triisopropyl-phenyl)-5-[2,4,6-tris-(bis-trimethylsilanyl-methyl)-phenyl]-[1,2,3,4,5]tetrathiasilolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 160359-05-7
(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)(dibromo)(2,4,6-triisopropylphenyl)silane

: 160359-06-8
5-(2,4,6-Triisopropyl-phenyl)-5-[2,4,6-tris-(bis-trimethylsilanyl-methyl)-phenyl]-[1,2,3,4,5]tetrathiasilolane

Guidance literature:: With sulfur; naphthalen-1-yl-lithium;
DOI:10.1021/ja00104a052

Reference yield:

: 162608-99-3
{2,4,6-tris[bis(trimethylsilyl)methyl]phenyl}silane

: 160359-06-8
5-(2,4,6-Triisopropyl-phenyl)-5-[2,4,6-tris-(bis-trimethylsilanyl-methyl)-phenyl]-[1,2,3,4,5]tetrathiasilolane

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / tetrahydrofuran / 10 h / -78 °C

2: 49 percent / NBS, benzoyl peroxide / benzene / 1 h / Heating

3: 1.) lithium naphthalenide, 2.) sulfur / 1.) THF, -78 deg C, 20 min, 2.) THF, -78 deg C, 10 min

With N-Bromosuccinimide; Perbenzoic acid; sulfur; naphthalen-1-yl-lithium; In tetrahydrofuran; benzene;
DOI:10.1021/ja980783c

Reference yield:

: 74226-59-8
2,4,6-triisopropylphenyl lithium

: 160359-06-8
5-(2,4,6-Triisopropyl-phenyl)-5-[2,4,6-tris-(bis-trimethylsilanyl-methyl)-phenyl]-[1,2,3,4,5]tetrathiasilolane

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / tetrahydrofuran / 10 h / -78 °C

2: 49 percent / NBS, benzoyl peroxide / benzene / 1 h / Heating

3: 1.) lithium naphthalenide, 2.) sulfur / 1.) THF, -78 deg C, 20 min, 2.) THF, -78 deg C, 10 min

With N-Bromosuccinimide; Perbenzoic acid; sulfur; naphthalen-1-yl-lithium; In tetrahydrofuran; benzene;
DOI:10.1021/ja980783c