C₁₃H₁₆O₃CH₄C₇H₆C₂H₄OC₅H₈OH₄SiC₆H₁₄PON₂C₄H₁₁

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Chemical Name:C₁₃H₁₆O₃CH₄C₇H₆C₂H₄OC₅H₈OH₄SiC₆H₁₄PON₂C₄H₁₁
CAS No.:331661-82-6
Molecular Formula:C₃₈H₆₇N₂O₆PSi
Molecular Weight:707.019
Hs Code.:

C<sub>13</sub>H<sub>16</sub>O<sub>3</sub>CH<sub>4</sub>C<sub>7</sub>H<sub>6</sub>C<sub>2</sub>H<sub>4</sub>OC<sub>5</sub>H<sub>8</sub>OH<sub>4</sub>SiC<sub>6</sub>H<sub>14</sub>PON<sub>2</sub>C<sub>4</sub>H<sub>11</sub>

Synonyms:C₁₃H₁₆O₃CH₄C₇H₆C₂H₄OC₅H₈OH₄SiC₆H₁₄PON₂C₄H₁₁

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Chemical Property of C₁₃H₁₆O₃CH₄C₇H₆C₂H₄OC₅H₈OH₄SiC₆H₁₄PON₂C₄H₁₁

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Technology Process of C₁₃H₁₆O₃CH₄C₇H₆C₂H₄OC₅H₈OH₄SiC₆H₁₄PON₂C₄H₁₁

There total 3 articles about C₁₃H₁₆O₃CH₄C₇H₆C₂H₄OC₅H₈OH₄SiC₆H₁₄PON₂C₄H₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1605-65-8
N,N,N',N'-Tetramethylphosphorodiamidic chloride

: 331627-46-4
(1R,4R,7R,8S,8aR)-1,2,3,4,6,7,8,8a-octahydro-4-benzyloxymethyl-4,7-dimethyl-8-tert-butyldimethylsilyloxymethyl-8-[2-(tetrahydro-2-pyranyloxy)ethyl]-1-naphthalenol

: 331661-82-6
C₁₃H₁₆O₃CH₄C₇H₆C₂H₄OC₅H₈OH₄SiC₆H₁₄PON₂C₄H₁₁

Guidance literature:: With N,N,N,N,-tetramethylethylenediamine; methyllithium; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1021/jo0015772

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 331661-82-6
C₁₃H₁₆O₃CH₄C₇H₆C₂H₄OC₅H₈OH₄SiC₆H₁₄PON₂C₄H₁₁

Guidance literature:: Multi-step reaction with 2 steps

1: 16.6 g / imidazole / dimethylformamide / 10 h / 20 °C

2: 93 percent / MeLi; TMEDA / tetrahydrofuran / 0 - 20 °C

With 1H-imidazole; N,N,N,N,-tetramethylethylenediamine; methyllithium; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo0015772

Reference yield:

: 331718-27-5
(1R,4R,7R,8S,8aR)-4-Benzyloxymethyl-8-hydroxymethyl-4,7-dimethyl-8-[2-(tetrahydro-pyran-2-yloxy)-ethyl]-1,2,3,4,6,7,8,8a-octahydro-naphthalen-1-ol

: 331661-82-6
C₁₃H₁₆O₃CH₄C₇H₆C₂H₄OC₅H₈OH₄SiC₆H₁₄PON₂C₄H₁₁

Guidance literature:: Multi-step reaction with 2 steps

1: 16.6 g / imidazole / dimethylformamide / 10 h / 20 °C

2: 93 percent / MeLi; TMEDA / tetrahydrofuran / 0 - 20 °C

With 1H-imidazole; N,N,N,N,-tetramethylethylenediamine; methyllithium; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo0015772